Method for preparing high-quality strontium carbonate
A strontium carbonate, high-quality technology, applied in the direction of calcium carbonate/strontium/barium, etc., can solve the trouble of synthesizing soda ash and other problems, and achieve the effects of good economic benefits, high equipment material requirements, and comprehensive cost reduction.
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Embodiment 1
[0021] Example 1. Mix celestite ore powder with a strontium sulfate content of 55-70% and reduced coal powder in a weight ratio of 1:1-1:1.5, and roast at a temperature of 1100-1200° C. for 4-5 hours to obtain black Ash, leaching three times in countercurrent with water to obtain leaching solution A and leaching residue a, and then leaching another part of black ash with leaching solution A countercurrently to obtain leaching solution B and leaching residue b, and using leaching solution B Leach the third part of black ash again to obtain leaching solution C and leaching residue c; combine leaching residues a, b, and c to be total leaching residues and stack them; obtained leaching solution C has a Sr content (calculated as SrS) of 50 ~200g / L yellow water.
[0022] Get 3 liters of yellow water containing SrS 153g / L, place in a batch reactor with stirring, add 136g industrial solid soda ash soda ash reaction (solid soda ash is added continuously by screw feeder), temperature of...
Embodiment 2
[0024] Example 2, mixing celestite ore powder with a strontium sulfate content of 55 to 70% and reduced coal powder in a weight ratio of 1:1 to 1:1.5, and roasting at a temperature of 1100 to 1200°C for 4 to 5 hours to obtain black Ash, leaching three times in countercurrent with water to obtain leaching solution A and leaching residue a, and then leaching another part of black ash with leaching solution A countercurrently to obtain leaching solution B and leaching residue b, and using leaching solution B Leach the third part of black ash again to obtain leaching solution C and leaching residue c; combine leaching residues a, b, and c to be total leaching residues and stack them; obtained leaching solution C has a Sr content (calculated as SrS) of 50 ~200g / L yellow water.
[0025] Get 3 liters of yellow water containing SrS 50g / L (0.4417mol / L) and place in a stirred batch reactor, then add 40% industrial liquid soda ash of 492mL to react (liquid soda ash is metered by a head t...
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