Method of forming a coating on a substrate, and a coating thus formed
A technology for substrates and coatings, applied in coatings, electrical components, circuits, etc., can solve the problems of high yield loss and achieve the effect of simple coating process
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[0037] Tetraethyl orthotitanate (TEOTi) was used as the matrix precursor component (yielding TiO 2 porous matrix), TiN particles as filler components, and then TEOTi (to produce TiO 2 ) as a precursor reinforcing component to prepare the porous protective coating according to the invention.
[0038] For this, 1 g of TEOTi was added to a solution of 0.3 g of HCl (6M) in 14.5 g of ethanol. To this solution was added 4.58 g of TiN to obtain a 4.4% by volume solution (thus obtaining 2 The porous matrix is 91% by volume of the filler component TiN).
[0039] To obtain a substantially uniform coating liquid, use ZrO 2 The grinding beads (2 mm diameter) were ground for 21 hours in a 60 ml PE-bottle and rotated at about 120 revolutions per minute (rpm). Added ZrO 2 The amount of beads is such that they are just below the surface of the coating liquid.
[0040] The resulting suspensions were sequentially deposited on glass substrates by spin coating. While the substrate was sp...
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