Neutral ink and its preparation method
A neutral ink, ink technology, applied in ink, household appliances, applications, etc., can solve the problems of large difference in viscosity measurement results, low scrap rate, small difference, etc.
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[0084] The preparation method of the ink is not particularly limited, as long as it does not limit the purpose of the invention.
[0085] In a specific embodiment of the present invention, it is prepared according to the following method:
[0086] (A) Add deionized water, anti-corrosion and anti-mold agent, moisturizing lubricant and viscosity stabilizing regulator into the container with a paddle stirrer in the order required by the formula measurement; after stirring evenly, slowly add shear Thin the viscosity modifier, and with the increase of viscosity, increase the stirring speed appropriately, when the system is evenly mixed; add the pigment paste, stir and mix for a certain period of time.
[0087] (B) Vacuum defoaming the ink prepared above, then centrifuging and filtering at high speed, collecting the filtrate for secondary defoaming to obtain the finished ink.
[0088] quality control method
[0089] The control index of the quality control method of the present in...
preparation Embodiment 1
[0101] 52.0 grams of deionized water, 0.5 grams of anticorrosion and antifungal agent (KathonLXE, benzotriazole purchased from Rohm and Haas, weight ratio is 1:1)) and 15 grams of ethylene glycol were added to the belt In a stirring tank with paddle stirring, mix evenly; under stirring, slowly add 2.5 grams of xanthan gum + Brunei gum (1:1 weight ratio), after adding, increase the stirring speed and stir evenly, and finally add black Pigment paste BayscriptBlack 30g. After continuing to stir and mix evenly, degassing—filtering—degassing to obtain the product.
[0102] The resulting product was rated as "good" in writing performance and had a shear thinning index of 3.0.
preparation Embodiment 2
[0104] 55.4 grams of deionized water, 0.2 grams of anti-corrosion and anti-fungal agent (Proxel XL2, benzotriazole purchased from United Kingdom Colloids Co., Ltd., the weight ratio of the two is 1:0.5), 10 grams of glycerin and 1.8 grams Add 2-methyl-2-amino-propanol into a stirring tank with paddle stirring, and mix evenly; under stirring, slowly add 4.6 grams of alkali-swellable acrylic acid emulsion (TT-615), after adding, increase After stirring evenly at a stirring speed, finally add 25 grams of Hostafine Blue and 3 grams of Bayscript Magenta into the pigment paste. After continuing to stir and mix evenly, degassing—filtering—degassing to obtain the product.
[0105] The resulting product was rated as "good" in writing performance and had a shear thinning index of 2.8.
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