Fluorocarbon compound modified polyacrylate flow agent for coating ink and production method thereof
A technology of fluorocarbons and polyacrylates, applied in the direction of coating, etc., can solve the problems of unsatisfactory working effect, complicated production process, and complicated raw materials, and achieve the effects of low production cost, increased surface gloss, and simple production methods
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Embodiment 1
[0021] (1) Xylene 1-10% (example 1%, 5%, 10%), toluene 1-10% (example 1%, 5%, 10%), propylene glycol methyl ether 1-20% (example 1%) , 19%, 20%) into the reactor, heated to 80 ~ 120 ℃ (for example 80 ℃, 100 ℃, 120 ℃);
[0022] (2) Add 30% to 70% of acrylate monomer (example 30%, 50%, 70%), initiator peroxide diphenyl ether (or azobisisobutyronitrile) 1% to 10% (example 1 %, 5%, 10%), acrylic acid fluorine monomer 1-20% (example 1%, 10%, 20%) at 80-150°C (example 80°C, 110°C, 150°C), 3- Put it into the above reaction kettle within 5 hours, keep it warm at 80-150°C (eg 80°C, 110°C, 150°C) for 2-5 hours to obtain the product.
[0023] The above-mentioned usage percentages are percentages by weight.
[0024] Wherein the acrylate monomer is methyl methacrylate (or butyl acrylate, etc.). The fluorine acrylate monomer is perfluoroalkyl acrylate (or nonadecafluoroheptyl acrylate, dodecafluoroheptyl methacrylate, hexafluorobutyl acrylate, etc.).
Embodiment 2
[0026] (1) Put xylene, toluene, and propylene glycol methyl ether into the reaction kettle, and heat up to 80-120°C (for example, 80°C, 100°C, 120°C);
[0027] (2) Add 30% to 70% of acrylate monomer (for example, 30%, 50%, 70%), initiator peroxydiphenyl ether (or azobisisobutyronitrile), acrylate fluorine monomer 1~20% (example 1%, 10%, 20%) at 80~150 ℃ (example 80 ℃, 110 ℃, 150 ℃), add in the above-mentioned reactor within 3~5 hours, 80~150 ℃ (example 80°C, 110°C, 150°C) for 2 to 5 hours to obtain the product.
[0028] Then add xylene to 1-10% (example 1%, 5%, 10%), toluene to 1-10% (example 1%, 5%, 10%), propylene glycol methyl ether to 1-20% ( Example 1%, 19%, 20%) and initiator diphenyl ether peroxide (or azobisisobutyronitrile) to 1-10% (example 1%, 5%, 10%), at 80-150°C Keep warm for 2-5 hours.
[0029] The above-mentioned usage percentages are percentages by weight.
[0030] Wherein the acrylate monomer is methyl methacrylate (or butyl acrylate, etc.). The fluorine...
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