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Preparation of alhagi sparsifolia total flavones and uses thereof

A technology of camel thorn and total flavonoids, which is applied in the field of extraction and separation of total flavonoids, and can solve the problems that the extraction and preparation process has not been reported yet.

Inactive Publication Date: 2008-09-10
XINJIANG TECHN INST OF PHYSICS & CHEM CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the process of studying camel thorns, the present invention finds that there are a large amount of flavonoids in camel thorns, but its extraction and preparation process has not been reported yet

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] a. Take 5 kg of the whole herb of Camel thorn, crush it into 6 meshes, add 10 times of ethanol with a concentration of 70%, and extract by conventional heating and reflux for 3 times, each time for 2 hours, keep the liquid surface slightly boiling, combine the filtrates, concentrate and dry;

[0017] b. Disperse the extract in an aqueous solution to prepare an aqueous solution, then put the AB-8 macroporous adsorption resin column on the aqueous solution, wash it with water until it is colorless, then wash it with 30% ethanol solution for 3 column volumes, collect, concentrate, That is the total flavonoids.

[0018] The camel thorn total flavonoids obtained by the method can be used for preparing medicine or as raw materials for preparing functional food, health care product or disinfection product.

Embodiment 2

[0020] a. Take 5 kg of the whole herb of Camel thorn, crush it into 6 meshes, add 15 times of methanol, extract twice by conventional soaking method, each time for 1 hour, combine the filtrate, concentrate and dry;

[0021] b. Disperse the extract in water to make an aqueous solution. The D101 macroporous adsorption resin column on the aqueous solution is first washed with water until it is colorless, then eluted with 35% ethanol of 4 times the column volume, concentrated under reduced pressure, and dried in vacuo to obtain total flavonoids.

[0022] The camel thorn total flavonoids obtained by the method can be used for preparing medicine or as raw materials for preparing functional food, health care product or disinfection product.

Embodiment 3

[0024] a. Take 5 kg of the whole herb of Camel thorn, grind it into 6 meshes, add 15 times of acetone, extract 3 times with conventional microwave-assisted method, each time for 1.5 hours, combine the filtrates, concentrate and dry;

[0025] b. Disperse the extract in water to make an aqueous solution. The D140 macroporous adsorption resin column on the aqueous solution is first washed with water until it is colorless, then eluted with 70% ethanol of 3 times the column volume, concentrated under reduced pressure, and dried in vacuo to obtain total flavonoids.

[0026] The camel thorn total flavonoids obtained by the method can be used for preparing medicine or as raw materials for preparing functional food, health care product or disinfection product.

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PUM

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Abstract

The invention discloses a method for manufacturing the total flavone of a camel thorn and the application thereof. By adopting the method, the camel thorn is extracted in organic solvent and then carries out the processes of macroporous polymeric absorbent column chromatography, elution in ethanol solution and concentration, so as to obtain the total flavone of the camel thorn. The total thorn can be taken as the constituent of gargle and disinfection products or used with other medicinal materials as the constituent of the gargle and the disinfection products.

Description

technical field [0001] The invention relates to a preparation method for extracting and separating total flavonoids from camel thorns. The total flavonoids from camel thorns obtained by the method can be used in medicine and hygiene, food and chemical industries, and the like. Background technique [0002] Camel thorn is a commonly used medicinal material in Uyghur medicine. The Uyghur name is Yantak, and it has a long history of medicine. "Compendium of Materia Medica", "Supplements to Compendium of Materia Medica", "Treasure House of Medicines" and so on all record sheep thorn, Gaochang tribute thorn honey, and sheep thorn honey. It is recorded in the literature that the dry leaves, flowers, seeds, whole plants and stem and leaf secretions (thorn sugar) of camel thorn can be used as medicine. The leaves are used to treat joint swelling and pain, the flowers are used to clear away heat and detoxify, the whole plant is used to treat colds and fever, damp heat in the stomach...

Claims

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Application Information

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IPC IPC(8): A61K36/48A61K8/97A61P1/16A61P9/00A61P29/00A61P35/00A61P39/06A61Q11/00A01N65/00A23L1/30
Inventor 阿吉艾克拜尔·艾萨苏小川
Owner XINJIANG TECHN INST OF PHYSICS & CHEM CHINESE ACAD OF SCI
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