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Quality control testing method for brain-invigorating and heart-soothing capsule

A detection method and capsule technology, applied in the field of pharmaceutical detection, can solve the problems of few detection methods and inability to guarantee drug detection, and achieve the effect of advanced detection methods, ensuring stability, uniformity, precision and reproducibility

Active Publication Date: 2010-12-22
JILIN AODONG YANBIAN PHARM CO LTD
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  • Abstract
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  • Application Information

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Problems solved by technology

[0003] The drug standard was originally recorded in the 18 volumes of standard Chinese medicine issued by the Ministry of Health. In the original standard, there were only TLC identifications of Polygonum multiflorum, Chuanxiong, and Chishao. Due to the lack of detection methods in the original standard, a comprehensive inspection of the drug cannot be guaranteed. detection

Method used

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  • Quality control testing method for brain-invigorating and heart-soothing capsule
  • Quality control testing method for brain-invigorating and heart-soothing capsule
  • Quality control testing method for brain-invigorating and heart-soothing capsule

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Experimental program
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Effect test

Embodiment 1

[0026] 1) Take 3g of the contents of Linaoxin Capsules, add 50ml of ether, soak for 30 minutes, filter, discard the ether solution, evaporate the dregs to dry the ether, add 50ml of 60% methanol, and ultrasonicate (power 250W, frequency 25KHz) for 20 minutes , filtered, evaporated to dryness, the residue was dissolved by adding 10ml of methanol, filtered, and the filtrate was concentrated to 0.5ml as the test solution; another 1g of licorice reference medicinal material was added, 20ml of methanol was added, and ultrasonic treatment (power 250W, frequency 25KHz) was performed for 20 Minutes, filter, evaporate to dryness, add 0.5ml of methanol to the residue to dissolve, and use it as a reference medicinal solution; test according to thin-layer chromatography, absorb 5 μl of each of the above two solutions, and spot on the same silica gel G prepared with 1% sodium hydroxide. On a thin-layer plate, use chloroform-ethyl acetate-acetone (5:2:1) as a developer, develop, take out, dr...

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Abstract

The invention discloses a quality controlling and testing method of a brain heart caring capsule, content determining by liquorice thin-layer chromatography identification and fleece-flower root efficient liquid chromatography method is added on the basis of the original testing standard. The testing method of the invention is advanced with excellent precision and reproducibility, can control thequality of the medicine comprehensively, and the stability and homogeneity of the quality of the product can be ensured.

Description

technical field [0001] The invention discloses a quality control detection method for Linaoxin capsules, which belongs to the technical field of medical detection methods. Background technique [0002] The "Linaoxin Capsule" involved in the present invention is made by the following process: decoct 40g of Danshen, 30g of Polygonum multiflorum (manufactured), 30g of Lycium barbarum, 30g of Radix Paeoniae Rubra, 30g of Radix Puerariae, and 30g of Earthworm in water for three times, and decoct three times for the first time. Hours, 2 hours for the second time, 1 hour for the third time, filter in stages, combine the filtrates, concentrate under reduced pressure into liquid extract, dry at low temperature, crush into fine powder, and set aside. Take 30g of Chuanxiong, 20g of safflower, 3g of turmeric, 30g of Alisma, 20g of jujube seed (stir-fried), 30g of polygala, 30g of iris calamus, 30g of Achyranthes bidentata, 20g of licorice, etc., and grind them into fine powder, sieve, a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N33/15G01N30/90A61K9/20A61K36/9066A61K35/64A61P9/10A61K35/62
Inventor 郭淑芹解钧秀于江波许加胜王永彬李伟
Owner JILIN AODONG YANBIAN PHARM CO LTD
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