Polyethylene molding compositions for injection molding applications
A molding composition, ethylene polymer technology, applied in the field of polyethylene molding composition for injection molding applications, can solve the problems of unsatisfactory, achieve good dimensional and shape stability, low shrinkage Effect
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[0215] Preparation of individual components
[0216] Bisindenyl zirconium dichloride and methylene bis(tetrahydroindenyl) zirconium dichloride are available from Crompton.
[0217] Carrier pretreatment
[0218] XPO-2107 (ie, spray-dried silica gel from Grace) was baked at 600°C for 6 hours.
example 1
[0220] Preparation of mixed catalyst systems
[0221] A mixture of 39.2 g of bisindenyl zirconium dichloride and 51.2 g of ethylene bis(tetrahydroindenyl) zirconium dichloride was dissolved in 5.2 l of MAO solution in toluene (4.75M in toluene, Albermarle) and stirred 60 minutes. While stirring, the solution was sprayed over 30 minutes onto 4 g of silica gel (XPO 2107, calcined at 600° C. for 6 hours). The line was rinsed with 0.5 1 of toluene. After stirring for an additional 1 hour at room temperature, the catalyst was packaged. 9.45 kg of catalyst system were obtained. The residual moisture content is 44.7% by weight based on the finished catalyst (based on the total weight and calculated on the total coating of all components on the support), the Al content is 6.1 g per 100 g of finished catalyst and the Zr content is 0.23 per 100 g of finished catalyst g.
[0222] polymerization
[0223] Ethylene-hexene copolymers were prepared using the catalyst system of Example 1...
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