Li-ion battery positive electrode material with layered-spinel symbiotic structure and preparation method
A technology for lithium-ion batteries and positive electrode materials, applied in electrode manufacturing, battery electrodes, structural parts, etc., can solve the problems of lack of cobalt resources and expensive materials, and achieve the solution of lack of cobalt resources, high capacity and cycle performance, and cost reduction Effect
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[0049] Example 1:
[0050] The product composition was designed with the mole ratio of Co, Ni, Mn = 0.2:0.2:0.6.
[0051] Material preparation: (x is a common coefficient in this example.) First, 0.4xmol of MnSO 4 .H 2 O is formulated into 2mol / L MnSO 4 solution, and then weigh 0.8x mol of NaOH to prepare a 2mol / L NaOH solution for the first precipitation. Weigh again 0.2x mol of CoSO 4 .7H 2 O, 0.2x mol NiSO 4 .6H 2 O and 0.2x mol of MnSO 4 .H 2 O was prepared into a mixed solution of 2 mol / L (Co+Ni+Mn); 1.2× mol of NaOH was weighed to prepare a 2 mol / L NaOH solution, which was used for the second co-precipitation. The complexing agent adopts ammonia water with a concentration of 0.36 mol / L.
[0052] making process:
[0053] First, add an appropriate amount of deionized water as the bottom liquid of the precipitation reaction in the reaction kettle, drop an appropriate amount of ammonia water and NaOH mixed solution to adjust the pH value of the bottom liquid to 10...
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[0059] Example 2:
[0060] The product composition was designed with the mole ratio of Co, Ni, Mn = 0.1:0.1:0.8.
[0061] Material preparation: (x is a common coefficient in this example.) First, 0.7x mol of MnSO 4 .H 2 O is configured as 2mol / L MnSO 4 solution; then weigh 0.14xmol of NaOH to prepare a 2mol / L NaOH solution for the first precipitation. Weigh again 0.1xmol of CoSO 4 .7H 2 O, 0.1x mol NiSO 4 .6H 2 O and 0.1xmol of MnSO 4 .H 2 O was prepared into a mixed solution of 2 mol / L (Co+Ni+Mn); 0.6× mol of NaOH was weighed to prepare a 2 mol / L NaOH solution, which was used for the second step of co-precipitation. The concentration of complexing agent ammonia water is 0.48mol / L.
[0062] making process:
[0063] First, an appropriate amount of deionized water was added to the reaction kettle as the bottom liquid of the precipitation reaction, and an appropriate amount of ammonia water and NaOH solution were added dropwise to adjust the pH value of the bottom liqu...
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