High silica/aluminum-based alloy and preparation method thereof
A technology of high-silicon-aluminum-based alloys, applied in the field of high-silicon-aluminum-based alloys and their preparation, can solve the problems of small and neglected thermal expansion coefficients, and achieve the effect of good electrical conductivity
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Embodiment 1
[0027] Pure Al and Si with a purity of not less than 99.5% are made into raw materials according to the required atomic percentage, and mixed rare earths with a Ce element content of 45% are prepared according to the required atomic percentage, and are produced in a vacuum induction melting furnace Prefabricated alloy Al-20Si-0.35Re; put the prefabricated alloy Al-20Si-0.35Re into a vacuum melting furnace, atomize and spray powder under the protection of argon-nitrogen, the melting temperature is 1000°C, and the protective pressure is 0.8MPa; Put the atomized alloy Al-20Si-0.35Re powder into a high-energy planetary ball mill with a ball-to-material ratio of 10:1, a ball milling speed of 700r / min, and a ball milling time of 6 hours, using alcohol protection for ball milling. A small amount of epoxy resin is added to the obtained powder with a particle size of about 10 μm to make the powder bond very tightly and increase the sintered density of the product. At a temperature of 3...
Embodiment 2
[0029] The technical solution is as in Example 1, and a high-silicon-aluminum-based alloy whose composition is Al-20Si-0.35Re is prepared. In this scheme, the milling time is 12 hours instead of 6 hours, and the pressure is 350MP instead of 300MP. A cuboid aluminum-based alloy with a length of 80 mm, a width of 40 mm and a thickness of 3 mm was prepared using the technical solution described in Example 1. The glass transition temperature (Tg) of the alloy is 795K, and the electrical conductivity of the alloy is measured by a bridge resistance meter, and the results are shown in the table below.
Embodiment 3
[0031] The technical solution is as in Example 1, and a high-silicon-aluminum-based alloy whose composition is Al-20Si-0.35Re is prepared. In this scheme, the milling time is 18h instead of 6h, and the pressure is 400MP instead of 300MP. A cuboid aluminum-based alloy with a length of 80 mm, a width of 40 mm, and a thickness of 3 mm was prepared using the technical solution described in Example 1. The electrical conductivity of the alloy was measured by a bridge-type resistance meter, and the results are shown in the table below.
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