Conductive silver ink for encapsulating LED and preparation method thereof
A technology of conductive silver glue and formula, applied in conductive adhesives, chemical instruments and methods, circuits, etc., can solve the problems of long curing time, waste, complicated construction process, etc., and achieve simple preparation method, environmental protection, energy consumption low effect
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[0032] A preparation method of conductive silver glue for encapsulating LEDs, mainly comprising the following steps:
[0033] 1) Weighing 5-25% glue matrix and 10-15% solvent respectively according to the composition and weight ratio;
[0034] 2) Mix the weighed resin with the solvent, and use a high-speed mixer to evenly disperse the resin in the solvent;
[0035] 3) Weighing 0.5-12% of the curing agent by weight and adding it to the mixed system of the above resin and solvent, using ultrasonic waves for 10-30 minutes, and controlling the temperature between 20-25°C to obtain the mixed system;
[0036] 4) Weighing 40-85% ultra-fine silver powder by weight and adding it to the above mixing system, stirring and dispersing with a defoaming mixer, so that the ultra-fine silver powder is fully dispersed in the organic system to obtain a preliminary conductive silver glue;
[0037] 5) weighing 0.05-10% curing accelerator by weight percentage for subsequent use;
[0038] 6) Weigh ...
Embodiment 1
[0041] A conductive silver glue for encapsulating LEDs, mainly comprising the following steps:
[0042] 1) Take by weighing 5% resin and 13% solvent, 60% ultrafine silver powder; 8% curing agent; 9.5% curing accelerator; 4.5% auxiliary agent according to the composition and weight percentage;
[0043] 2) Mix the weighed resin and the solvent together, make the high-speed mixer stir for 15 minutes under the condition of 1200rpm, and evenly disperse the resin in the solvent;
[0044] 3) Weigh 8% curing agent HB-175 by weight percentage and add it to the mixed system of the above resin and solvent, perform ultrasonic treatment for 30 minutes, and control the temperature between 25°C to obtain the mixed system;
[0045] 4) 60% of the ultra-fine silver powder weighed by weight is added to the above mixing system, stirred and dispersed with a defoaming mixer for 10 minutes, so that the ultra-fine silver powder is fully dispersed in the organic system, and a preliminary conductive si...
Embodiment 2
[0050] A preparation method of conductive silver glue for encapsulating LEDs, mainly comprising the following steps:
[0051] 1) Take by weighing 10% glue base and 11% ethylene glycol diethyl ester solvent, 77% ultrafine silver powder; 0.5% curing agent; 1% curing accelerator; 0.5% Auxiliary;
[0052] 2) Mix the weighed resin and the solvent together, make the high-speed mixer stir for 15 minutes under the condition of 1200rpm, and evenly disperse the resin in the solvent;
[0053] 3) Weigh 0.5% curing agent SM-75L by weight percentage and add it to the mixed system of the above resin and solvent, perform ultrasonic treatment for 10 minutes, and control the temperature between 20°C to obtain the mixed system;
[0054] 4) 77% of the ultra-fine silver powder weighed by weight is added to the above mixing system, stirred and dispersed with a defoaming mixer for 15 minutes, so that the ultra-fine silver powder is fully dispersed in the organic system, and a preliminary conductive...
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