Method for extracting volatile oil from Ziziphora Clinopodioides Lam herb by CO2 supercritical extraction technique

An extraction technology, a new tower flower technology, is applied in the field of extracting volatile oil of active components, which can solve the problems of high energy consumption and long time, and achieve the effects of simple extraction process, stable gas source and high extraction efficiency.

Inactive Publication Date: 2009-09-09
新疆新绿宝药业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The current technology is to extract the volatile oil from the whole plant of Xintahua, which mostly uses steam distillation, which has the disadvantages of long existence time, high energy consumption, and a small amount of water residue in the product.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Take 100g of the whole grass of Xintahua, wash it, dry it at room temperature, pulverize it with a pulverizer, and pass it through a 40-mesh sieve to obtain the whole grass of Xintahua powder;

[0020] Turn on the power supply of the supercritical extraction equipment, turn on the cold cycle switch and the heating switch, the temperature of the extraction cylinder is 35°C, the temperature of the separation cylinder I is 30°C, and the temperature of the separation cylinder II is 20°C;

[0021] Put Xintahua whole grass powder into the extraction tank and start the CO 2 Circulation system, adjust the pressure of the extraction cylinder to 10MPa, the pressure of the separation cylinder I to 6MPa, and the pressure of the separation cylinder II to 3MPa;

[0022] Start timing when the temperature and pressure of the extraction cylinder, separation cylinder I and separation cylinder II reach the set value;

[0023] After 60 minutes of extraction, volatile oil was released from...

Embodiment 2

[0025] Take 100g of the whole grass of Xintahua, wash it, dry it at room temperature, pulverize it with a pulverizer, and pass it through a 40-mesh sieve to obtain the whole grass of Xintahua powder;

[0026] Turn on the power supply of the supercritical extraction equipment, turn on the cold circulation switch, and the heating switch, the temperature of the extraction cylinder is 40 °C, the temperature of the separation cylinder I is 30 °C, and the temperature of the separation cylinder II is 20 °C;

[0027] Put Xintahua whole grass powder into the extraction tank and start the CO 2 Circulation system, adjust the pressure of extraction cylinder to 15MPa, the pressure of separation cylinder I to be 6MPa, and the pressure of separation cylinder II to be 3MPa;

[0028] Start timing when the temperature and pressure of the extraction cylinder, separation cylinder I and separation cylinder II reach the set value;

[0029] After 90 minutes of extraction, volatile oil was released ...

Embodiment 3

[0031] Take 100g of the whole grass of Xintahua, wash it, dry it at room temperature, pulverize it with a pulverizer, and pass it through a 40-mesh sieve to obtain the whole grass of Xintahua powder;

[0032] Turn on the power supply of the supercritical extraction equipment, turn on the cold cycle switch and the heating switch, the temperature of the extraction cylinder is 45°C, the temperature of the separation cylinder I is 30°C, and the temperature of the separation cylinder II is 20°C;

[0033] Put Xintahua whole grass powder into the extraction tank and start the CO 2 Circulation system, adjust the pressure of extraction cylinder to 20MPa, the pressure of separation cylinder I to 6MPa, and the pressure of separation cylinder II to be 3MPa;

[0034] Start timing when the temperature and pressure of the extraction cylinder, separation cylinder I and separation cylinder II reach the set value;

[0035] After 120 minutes of extraction, volatile oil was released from the dis...

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PUM

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Abstract

The invention relates to a method for extracting volatile oil from Ziziphora Clinopodioides Lam herb by CO2 supercritical extraction technique, comprising the steps of: cleaning and drying the Ziziphora Clinopodioides Lam herb at normal temperature, disintegrating by a disintegrator, sieving to obtain Ziziphora Clinopodioides Lam herb powder, putting the Ziziphora Clinopodioides Lam herb powder in an extraction cylinder for extraction, and then discharging the volatile oil through discharging holes of a separation cylinder I and a separation cylinder II. The invention, in no need of any solvent, can be implemented at normal temperature with CO2 being non-toxic and residual-free, and the invention is low in energy consumption, stable in gas source, recyclable, simple in extraction technology and high in extraction efficiency; the yield of the volatile oil thereof can run up to over 1.8%. The invention overcomes the disadvantages that the traditional steam distillation method used for extracting the volatile oil from the Ziziphora Clinopodioides Lam wastes a lot of time and energy and residual moisture is present in the product.

Description

technical field [0001] The invention relates to a method for extracting the volatile oil of effective components from the whole grass of Xintahua plant. Background technique [0002] Z bungeana Juz (Z bungeana Juz) is a sub-shrub herb with a strong mint fragrance. It is mainly produced in the Altai Mountains, Tianshan Mountains, Western Junggar Mountains, Pamirs and Kunlun Mountains in Xinjiang. Mountain grasslands and gravel slopes are also distributed in Central Asia and Mongolia. Fragrant new tower flower is a folk Chinese herbal medicine and a commonly used national medicine. It is called Xuze or Suze in Xinjiang Uyghur medicine. It is mainly used for the treatment of hypertension and coronary heart disease and to regulate the function of the cardiovascular system. Its active ingredients are mainly volatile oil, Flavonoids, alkaloids and vitamin C and other ingredients. [0003] Twenty-nine chemical constituents were identified from the volatile oil of Aromaxinta flowe...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/53A61P9/10A61P9/12A61P9/00A23L1/29C11B1/10A23L33/00
Inventor 阿吉艾克拜尔·艾萨史昊阿依古丽·塔西阿不都吾甫尔·热依木古丽
Owner 新疆新绿宝药业有限公司
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