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Method and device for preparing continuous cylindrical crystalline texture high-silicon electrical steel bar

A high-silicon electrical steel and columnar crystal technology is applied in the field of devices for preparing high-silicon electrical steel bars with continuous columnar crystal structure, and can solve the problem of difficulty in preparing high-silicon electrical steel bars, poor thermal conductivity and thermal conductivity of high-silicon electrical steel. Insufficient and other problems, to meet the requirements of subsequent processing and performance, improve the efficiency of vacuuming, and reduce the effect of high temperature reaction

Inactive Publication Date: 2009-12-30
UNIV OF SCI & TECH BEIJING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, the composition and impurity control requirements of high-silicon electrical steel are strict, the melting point is high (over 1400 ° C), and Si is relatively active at high temperature, and it is easy to react with the crucible; at the same time, high-silicon electrical steel has poor thermal conductivity (such as 6.5% The thermal conductivity of Si silicon steel is less than 1 / 10 of that of pure copper), so it is difficult to prepare large-sized and continuous columnar crystals with existing directional solidification equipment and processes (such as exothermic agent method, high-speed solidification method, and continuous directional solidification method). Tissued High Silicon Electrical Steel Rods

Method used

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  • Method and device for preparing continuous cylindrical crystalline texture high-silicon electrical steel bar
  • Method and device for preparing continuous cylindrical crystalline texture high-silicon electrical steel bar
  • Method and device for preparing continuous cylindrical crystalline texture high-silicon electrical steel bar

Examples

Experimental program
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Effect test

Embodiment 1

[0030] Example 1: Fe-6.5Si-0.05B ​​high-silicon steel bar with a diameter of 20 mm and a length of 300 mm.

[0031]The Fe-6.5Si-0.05B ​​high-silicon steel alloy is melted in a medium-frequency vacuum induction furnace and cast into ingots. The raw materials are rod-shaped pure iron (99.9%), block-shaped metal silicon (99.9%) and block-shaped ferroboron (the total content of iron and boron is 99.95%, and boron content is 17.5%). High-silicon steel rods with a diameter of 20mm and a length of 300mm were prepared under the process scheme of high-frequency power supply frequency 450kHz, power 40kW, melt temperature 1500°C, cooling water flow rate of about 15L / min, and traction speed of 2mm / min. . The surface of the prepared bar is relatively bright, the internal structure is continuous columnar grain structure, and the diameter of the columnar grain is about 1000 μm. image 3 , as shown in 4.

[0032] X-ray diffraction experiments were carried out on the cross section of the ba...

Embodiment 2

[0033] Example 2: Fe-6.5Si-0.05B ​​high-silicon steel bar with a diameter of 6 mm and a length of 200 mm.

[0034] The Fe-6.5Si-0.05B ​​high-silicon steel alloy is melted in a medium-frequency vacuum induction furnace and cast into ingots. The raw materials are rod-shaped pure iron (99.9%), block-shaped metal silicon (99.9%) and block-shaped ferroboron (the total content of iron and boron is 99.95%, and boron content is 17.5%). High-silicon steel rods with a diameter of 6mm and a length of 200mm were prepared under the process scheme of high-frequency power supply frequency 600kHz, power 15kW, melt temperature 1450°C, cooling water flow rate of about 10L / min, and traction speed of 10mm / min. The surface of the prepared rod is relatively bright, and the internal structure and X-ray diffraction results are similar to those of Example 1, all of which are columnar crystal structures.

Embodiment 3

[0035] Example 3: Fe-6.5Si-0.05B ​​high-silicon steel bar with a diameter of 50 mm and a length of 500 mm.

[0036] The Fe-6.5Si-0.05B ​​high-silicon steel alloy is melted in a medium-frequency vacuum induction furnace and cast into ingots. The raw materials are rod-shaped pure iron (99.9%), block-shaped metal silicon (99.9%) and block-shaped ferroboron (the total content of iron and boron is 99.95%, and boron content is 17.5%). High-silicon steel rods with a diameter of 50mm and a length of 500mm were prepared under the process scheme of high-frequency power supply frequency 600kHz, power 15kW, melt temperature 1550°C, cooling water flow rate of about 20L / min, and traction speed of 0.5mm / min. . The surface of the prepared rod is relatively bright, and the internal structure and X-ray diffraction results are similar to those of Example 1, all of which are columnar crystal structures.

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Abstract

The invention relates to a method and a device for preparing a continuous cylindrical crystalline texture high-silicon electrical steel bar. The method comprises the following steps: metal blank under the protection of inert gas in a crucible melts under the action of alternating magnetic field formed by high-frequency induction coils, simultaneously a static magnetic field generator forms a magnetic field parallel to the direction of directional solidified hot flow in melt, and a cooling system forms a temperature gradient along the pulling direction in solidified metal and unsolidified melt so as to lead the melt to be solidified to form the cylindrical crystalline texture. Under the effect of a feeding and pulling mechanism, the above solidifying process is carried out continuously, thus obtaining the blank with the continuous cylindrical crystalline texture. In the the invention, a mode of combining zone melting and secondary water cooling is adopted, the directional solidifying preparation of the high-silicon electrical steel cylindrical bar with the maximum diameter of 50mm and the maximum of 800mm can be met by utilizing the effect of the static magnetic field, and simultaneously the invention has the characteristics of simple mechanism, easy monitoring of melt temperature and the like.

Description

Technical field: [0001] The invention belongs to the technical field of material preparation, and in particular provides a device and a process for preparing high-silicon electrical steel rods with continuous columnar crystal structure. Background technique: [0002] Electrical steel (also known as silicon steel) is mainly used in iron cores of various motors and transformers and other electrical products, and is an indispensable soft magnetic alloy for electric power, electronics and military industries. Especially grain-oriented electrical steel, due to its excellent magnetic properties, is a key material for high-performance, low-loss, low-noise transformers and other devices. Due to the complex production process of grain-oriented electrical steel, strict requirements on composition and impurity control, etc., it is called "special steel art" [Yu Yongmei, Li Changsheng, Wang Guodong. Research on the technology of thin slab continuous casting and rolling to produce grain-...

Claims

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Application Information

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IPC IPC(8): B22D27/02
Inventor 张志豪付华栋谢建新
Owner UNIV OF SCI & TECH BEIJING