Method for removing excessive citrate contained in gold-plating solution
A technology of citrate and electroplating gold, which is applied in the direction of electrolysis process, electrolysis components, cells, etc. It can solve the problems of dark coating, difference in thickness, and lower upper limit of current density, etc., and achieve the effect of low cost and simple operation
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example 1
[0037] The formulation of the plating solution adopts commercially available potassium gold citrate products without inorganic free cyanide and Technic electroplating thick gold additives. The process formula is as follows:
[0038] Potassium gold citrate 22g / L; conductive salt 90g / L; auxiliary salt 45g / L; adjusting salt 30g / L; brightener A: 2ml / L; B: 10ml / L pH=4.5; temperature 50°C; D K 15A / dm 2 .
[0039] According to the above process conditions, the coating is yellow and bright. Add potassium citrate 100g / L, the high current density area of the coating will be severely burnt, and the coating will be dark in the low current density area. Adding brightener has no effect. According to the treatment method in the present invention, the pH value is adjusted with hydrochloric acid; 8g / L of hexamethylenetetramine and 54g / L of calcium chloride are added at one time, and an appropriate amount of brightener is added to the regenerated gold plating solution after filtration, an...
example 2
[0041] The process formula is as follows:
[0042] Gold Potassium Citrate 20g / L; Potassium Citrate 150g / L; Potassium Dihydrogen Phosphate 25g / L; Citric Acid 40g / L; Brightener 10ml / L; pH=4.5; K 15A / dm 2 .
[0043] According to the above process conditions, the coating is yellow and bright. Add potassium citrate 100g / L, the high current density area of the coating will burn severely, and the coating will become dark in the low current density area. Adding brightener has no effect. According to the treatment method in the present invention, adjust the pH value with hydrochloric acid; add hexamethylenetetramine 6g / L, calcium carbonate consumption 50g / L at one time, add brightener to the regenerated gold plating solution after filtration, and the coating quality returns to normal.
[0044] The above-mentioned aqueous solution of calcium-containing substances mainly refers to an aqueous solution of calcium salt.
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