Method for extracting ginseng, dwarf lilyturf tuber and schisandra chinensis and preparation thereof
The technology of Schisandra chinensis and Ophiopogon japonicus is applied in the field of preparations for nourishing Qi and Fumai for treating cardiovascular diseases and the preparation thereof, which can solve the problems of low extraction rate, high cost, complicated production process and the like, and achieves high extraction rate, low cost and curative effect. high effect
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Embodiment 1
[0065] (1) Combined extraction of Ophiopogon japonicus and Schisandra chinensis, the extraction steps are as follows:
[0066] (1) Take the Ophiopogon japonicus and Schisandra chinensis of the prescription amount, reflux with water, and reflux twice with 4 times the water, each time for 30 minutes;
[0067] (2) The water extract was passed through D101 resin, eluted with 50% ethanol, concentrated to a relative density of 1.03-1.10 after decolorization, and filtered;
[0068] (3) The eluate obtained in step (2) is refrigerated, filtered, and concentrated to obtain an extract, which is a composite extract;
[0069] (2) Ginseng is extracted separately, and the extraction steps are as follows:
[0070] Add 8 times the amount of 80% ethanol to ginseng coarse powder, soak for 12 hours, put it into ultrasonic extraction, power 100W, temperature 30°C, solvent volume 8 times, extract 3 times, 20 minutes each time, wave off the ethanol to obtain a single extract ;
[0071] The above ...
Embodiment 2
[0073] (1) Combined extraction of Ophiopogon japonicus and Schisandra chinensis, the extraction steps are as follows:
[0074] (1) Take the Ophiopogon japonicus and Schisandra chinensis of the prescription amount, reflux with water, 10 times of water reflux 3 times, each time for 2 hours;
[0075] (2) The water extract was passed through D4020 resin, washed with water, then eluted with 80% ethanol, concentrated to a relative density of 1.03-1.10 after decolorization, and filtered;
[0076] (3) The eluate obtained in step (2) is refrigerated, filtered, and concentrated to obtain an extract, which is a composite extract;
[0077] (2) Ginseng is extracted separately, and the extraction steps are as follows:
[0078] Add 3 times the amount of 50% ethanol to ginseng coarse powder, soak for 12 hours, put it into ultrasonic extraction, power 100W, temperature 30°C, solvent volume 8 times, extract 3 times, 20 minutes each time, wave off the ethanol to obtain a single extract ;
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Embodiment 3
[0081] (1) Combined extraction of Ophiopogon japonicus and Schisandra chinensis, the extraction steps are as follows:
[0082] (1) Take the Ophiopogon japonicus and Schisandra chinensis of the prescription amount, reflux with water, 6 times of water reflux 3 times, each time for 1 hour;
[0083] (2) The water extract is passed through D4020 macroporous adsorption resin, washed with water, then eluted with 70% ethanol, concentrated to a relative density of 1.03-1.10 after decolorization, and filtered;
[0084] (3) The eluate obtained in step (2) is refrigerated, filtered, and concentrated to obtain an extract, which is a composite extract;
[0085] (2) Ginseng is extracted separately, and the extraction steps are as follows:
[0086] Add 8 times the amount of 80% ethanol to ginseng coarse powder, soak for 12 hours, put it into ultrasonic extraction, power 100W, temperature 30°C, solvent volume 8 times, extract 3 times, 20 minutes each time, wave off the ethanol to obtain a sin...
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