High temperature resistance diaphragm-controlled phytase pellets and preparation method thereof
A technology of phytase pellets and high temperature resistant film, applied in application, animal feed, animal feed, etc., can solve the problems of processing requirements, unsatisfactory thermal stability, etc., to achieve improved enzyme activity retention rate, good dispersibility, The effect of high enzymatic activity
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The preparation method of the high temperature resistant membrane-controlled phytase pellets of the present invention firstly adopts the extrusion spheronization method to prepare the phytase pellet core, and then uses the bottom spray fluidized bed to prepare the phytase pellets into coated pellets . include:
Step 1: Slowly add stabilizer and anti-sticking agent to the phytase fermentation broth under stirring, sieve and mix the auxiliary materials, and then mix the phytase fermentation broth and auxiliary materials to make a soft material;
Step 2: Place the soft material in an extrusion spheronization machine to extrude and spheronize to make a phytase pellet core;
(3) Prepare three layers of coating liquid separately, that is, slowly add the coating material to the water under stirring conditions and mix evenly. Take an appropriate amount of phytase pellets and place them in the fluidized bed, spray them evenly, and fluidize the pellets in the fluidized bed for 20-40 minut...
Example Embodiment
Example 1:
Phytase pellet preparation
Preparation of soft material: slowly add 5% sodium sulfate to the phytase fermentation broth under stirring, sieve and mix the auxiliary materials 100g corn starch and 150g white carbon black, and then mix the phytase fermentation broth and auxiliary materials to make a soft Material, spare.
Extrusion spheronization: Put the soft material in the extruder and adjust the extrusion speed. After all the elongated extrudates fall into the spheronizer, the spheronization starts. Adjust the appropriate spheronization speed. The spheronization time is 3-15 minutes. .
Preparation of phytase coated pellets
Water-soluble water-absorbing coating layer: 50 mL of 1% polyvinylpyrrolidone aqueous solution, which contains 30% potassium chloride and an appropriate amount of talc.
Water-soluble heat-stable coating layer: xanthan gum 5g, prepared into a solution with water, and set aside.
Fat-soluble water-blocking coating layer: EudragitRL / RS solution 45...
Example Embodiment
Example 2:
Preparation of phytase coated pellets
Preparation of soft materials: slowly add 4% magnesium sulfate to the phytase fermentation broth under stirring, sieve and mix the auxiliary materials 100g microcrystalline cellulose, 30g white carbon black, and 70g maltodextrin, and then mix the phytase fermentation broth Mix evenly with auxiliary materials to make soft material for use.
Extrusion spheronization: Put the soft material in the extruder and adjust the extrusion speed. After all the elongated extrudates fall into the spheronizer, the spheronization starts. Adjust the appropriate spheronization speed. The spheronization time is 3-15 minutes. .
Preparation of phytase coated pellets
Water-soluble water-absorbing coating layer: 40 mL of 1% polyvinylpyrrolidone aqueous solution, which contains 15% zinc sulfate, and an appropriate amount of finely powdered silica gel.
Water-soluble heat-stable coating layer: 6g gum arabic, prepared as a solution with water, for use.
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