Phenolic resin and preparation method thereof
A technology of phenolic resin and phenol, applied in the field of phenolic resin and preparation, can solve the problems of increasing the greenhouse effect, excessive moisture content in semi-finished products, etc., and achieves the effects of increasing economic benefits, lowering costs, and reducing emissions
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Embodiment 1
[0017] Raw materials
[0018] Phenol: industrial product (99.5%) produced by Yanshan Petrochemical Industry Group Corporation
[0019] Formaldehyde: industrial product (37.0%) produced by Shandong Lunan Fertilizer Plant
[0020] NaOH solution: (50%) self-made
[0021] Paraformaldehyde: industrial products (95%) Weifang Huifeng Chemical Co., Ltd.
[0022] equipment
[0023] 3000L reactor, supporting condensing device, stirring, vacuum pump device.
[0024] Raw material formula:
[0025] Phenol 1000kg Formaldehyde 150kg 50% NaOH 20kg Paraformaldehyde 450kg
[0026] Craft
[0027] Feeding is carried out in sequence during the stirring process. Firstly, 1000 kg of preheated molten phenol is sucked into the reactor in a vacuum, and then 20 kg of 50% NaOH catalyst is added. The temperature is raised to 80°C, and 150 kg of formaldehyde is added at 80°C to perform polycondensation reaction and heat preservation. React for 0.5 hours, add 450kg of paraformaldehyde in 4 batches, keep the temperature f...
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