Rare earth polishing powder and production method thereof

A technology of rare earth polishing powder and manufacturing method, which is applied in the direction of chemical instruments and methods, and other chemical processes, and can solve the problems of slow polishing speed and poor polishing effect

Active Publication Date: 2010-12-01
甘肃稀土新材料股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Since the second half of 2006, the domestic crystal lighting balls, rhinestones, and ironing diamond industries have developed very rapidly, and the amount of polishing powder in this industry has also increased rapidly. However, the application of conventional rare earth polishing powder in this industry has slow polishing speed, Poor polishing effect and other shortcomings, the total amount of rare earth in rare earth polishing powder is generally 88wt%-90wt%, the content of cerium oxide CeO2 accounts for 60wt%-70wt% of the total amount of rare earth oxide TREO, lanthanum oxide La 2 o 3 Content in the proportion of total rare earth oxides TREO 25wt%-35wt%, praseodymium oxide Pr 6 o 11 The content of TREO accounts for 5wt%-10wt% of the total amount of rare earth oxides, neodymium oxide Nd 2 o 3 The proportion of the content in the total amount of rare earth oxides TREO is less than 0.2wt%; the proportion of fluorine F in the total amount of rare earth oxides TREO accounts for 3wt%-5wt%

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0017] First prepare the rare earth chloride liquid raw material with less neodymium, the total amount of rare earth in its rare earth polishing powder TREO, cerium oxide CeO 2 The proportion of content accounts for 70-80%, lanthanum oxide La 2 o 3 The proportion of content accounts for 19-29%, praseodymium oxide Pr 6 o 11 The content ratio is 0.05-2%, neodymium oxide Nd 2 o 3 The proportion of content is 0.2%. Neutralizing agent ammonia NH 3 h 2 0 regulates the pH value of raw material liquid to 4.5, carries out plate-and-frame filter press filter then, removes the non-rare earth impurities such as thorium, iron, puts into storage tank for subsequent use; The content that will prepare is the little neodymium chloride rare earth liquid of 205g / L 650L, 12L of silicofluoric acid with a content of 40% and 25L of an ammonium sulfate additive with a content of 50% are put into the enamel stirring tank, and after being fully stirred evenly, the temperature is raised to 85°C t...

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PUM

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Abstract

The invention discloses rare earth polishing powder and a production method thereof. As an abrasive substance, the polishing powder comprises CeO2, La2O3 and Pr6O11. The total rare earth oxides (TREO) are above 90wt%. Meanwhile, in the TREO of the 877-3 rare earth polishing powder, CeO2 accounts for 70-80%, La2O3 19-29%, Pr6O11 0.05-2% and Nd2O3 less than 0.2%. To ensure necessary polishing speed, fluorine element which has chemical action is added to the wet synthesis process and initial shaping of product granularity is controlled, so that the obtained 877-3 rare earth polishing powder can be used for fast producing polished surface with good polishing effect.

Description

technical field [0001] The invention belongs to the field of rare earth product preparation, in particular to a rare earth polishing powder and a manufacturing method thereof. Background technique [0002] Since the second half of 2006, the domestic crystal lighting balls, rhinestones, and ironing diamond industries have developed very rapidly, and the amount of polishing powder in this industry has also increased rapidly. However, the application of conventional rare earth polishing powder in this industry has slow polishing speed, Poor polishing effect and other shortcomings, the total amount of rare earth in rare earth polishing powder is generally 88wt%-90wt%, the content of cerium oxide CeO2 accounts for 60wt%-70wt% of the total amount of rare earth oxide TREO, lanthanum oxide La 2 o 3 Content in the proportion of total rare earth oxides TREO 25wt%-35wt%, praseodymium oxide Pr 6 o 11 The content of TREO accounts for 5wt%-10wt% of the total amount of rare earth oxides...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K3/14
Inventor 任立华杨文浩高国勤赵军李友兴马相琴
Owner 甘肃稀土新材料股份有限公司
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