Nonmagnetic hard alloy and preparation method
A cemented carbide and non-magnetic alloy technology, which is applied in the field of non-magnetic cemented carbide materials and preparation, can solve the problems of easy cracking, bending deformation, and difficulty in controlling the carbon content of the alloy, and achieves high control accuracy and no sintering cracks. , the effect of small bending deformation
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Embodiment 1
[0021] Example 1: Prepare a single weight 50Kg non-magnetic hard alloy (outer diameter: 411 mm), the composition and weight percentage are: nickel: 12%, chromium carbide: 1.2%, tungsten carbide: balance.
[0022] The preparation of the above-mentioned non-magnetic hard alloy includes raw material preparation, wet grinding, drying, pressing, sintering and other processes (the following examples are the same). The raw material composition and weight percentage are: nickel powder: 12%, chromium carbide powder 1.2%, tungsten carbide powder balance. Weigh each raw material in proportion, add molding agent, ball mill the prepared mixture in a wet mill, spray dry at a drying temperature of 90-100°C, and then press it into a green compact of specified size and shape, then put it into dewaxing and sintering In the integrated furnace, hydrogen gas with a dew point of -60°C is introduced, and the furnace temperature is raised from room temperature to 550°C within 40 to 45 hours to comple...
Embodiment 2
[0023] Example 2: Prepare a single weight 30Kg non-magnetic hard alloy (outer diameter: 380mm), the composition and weight percentage are: nickel: 11%, chromium carbide: 0.75%, tungsten carbide: the balance.
[0024] Raw material composition and weight percentage are: nickel powder: 11%, chromium carbide powder: 0.75%, tungsten carbide powder: balance. Weigh each raw material in proportion, add molding agent, ball-mill the prepared mixture in a wet mill, and then spray dry at a drying temperature of 90-100°C, then press it into a compact of specified size and shape, and put it into dewaxing In the integrated sintering furnace, hydrogen gas with a dew point of -60°C is introduced, and the furnace temperature is raised from room temperature to 500°C within 35 to 40 hours; then the temperature is raised again within 8 to 9 hours until the product appears in a liquid phase, and the pressure in the furnace at this stage is ≤ 0.8mbar; after the liquid phase appears, fill the furnace...
Embodiment 3
[0025] Example 3: Prepare a single weight 10Kg non-magnetic hard alloy (outer diameter: 212mm), the composition and weight percentage are: nickel: 10%, chromium carbide: 1.0%, tungsten carbide: balance.
[0026] The raw material composition and weight percentage are: nickel powder: 10%, chromium carbide powder: 1.0%, tungsten carbide powder: balance. Weigh each raw material in proportion, add molding agent, ball-mill the prepared mixture in a wet mill, and then spray dry at a drying temperature of 90-100°C, then press it into a compact of specified size and shape, and put it into dewaxing In the integrated sintering furnace, hydrogen gas with a dew point of -60°C is introduced, and the furnace temperature is raised from room temperature to 450°C within 25 to 35 hours to complete the removal of the forming agent; At this stage, the pressure in the furnace is ≤0.8mbar; after the liquid phase appears, fill the furnace with about 40mbar of high-purity argon gas with a volume perce...
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