Water soluble low-temperature-solidification appliance insulating varnish and preparation method thereof

An insulating varnish, water-soluble technology, applied in the direction of coating, etc., can solve the problems of not being able to withstand the baking temperature above 100 ℃, high baking and curing temperature, multi-energy, etc., to achieve energy saving, strong paint film adhesion, The effect of improving the performance of the paint film

Inactive Publication Date: 2010-12-29
深圳市东方亮化学材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The defect of the prior art is that the baking and curing temperature is too high, which not only consumes more energy, but also many electrical products cannot withstand the baking temperature above 100°C at all.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] Embodiment 1: formula composition is as follows:

[0042] 1. Ethyl acrylate 35.0kg

[0043] 2. Silicone resin 15.0kg

[0044] 3. Diethylene glycol 4.0kg

[0045] 4. Diethanolamine 1.0kg

[0046] 5. Benzoyl peroxide 0.5kg

[0047] 6. Amino resin INEOS747 3.0kg

[0048] 7. Silicone oil 0.4kg

[0049] 8. BYK028 0.2kg

[0050] 9. Deionized water 40.9kg

[0051] Stir slowly at room temperature, mix the components ethyl acrylate, silicone resin, diethylene glycol, benzoyl peroxide and 50% deionized water evenly, and stir for about 20 minutes; then add BYK028, amino resin INEOS747 in sequence , silicone oil and the remaining deionized water, and continue to stir for 20 minutes; then slowly add diethanolamine dropwise, adjust the pH to the range of 8.0-9.0, and the finished product can be obtained. It can be used as impregnating insulating varnish for transformers, micro-motors, coils, etc. The temperature of baking and curing film formation is 80-90°C, and the baking t...

Embodiment 2

[0053] The preparation process is the same as in Example 1, but the material and content of each component change to as follows:

[0054] 1. Octyl acrylate 32.0kg

[0055] 2. Silicone resin 10.0kg

[0056] 3. Ethylene glycol 6.0kg

[0057] 4. Monoethanolamine 1.2kg

[0058] 5. Benzoyl peroxide 1.0kg

[0059] 6. Amino resin INEOS747 3.5kg

[0060] 7. Polyether modified silicone oil 0.6kg

[0061] 8. BYK028 0.30kg

[0062] 9. Deionized water 45.4kg

[0063] The preparation process is the same as in Example 1.

Embodiment 3

[0065] The preparation process is the same as in Example 1, but the material and content of each component change to as follows:

[0066] 1. Butyl acrylate 38.0kg

[0067] 2. Silicone resin 12.0kg

[0068] 3. Glycerol 5.0kg

[0069] 4. Triethanolamine 1.0kg

[0070] 5. Benzoyl peroxide 0.8kg

[0071] 6. Amino resin INEOS747 2.5kg

[0072] 7. Silicone oil 0.5kg

[0073] 8. BYK347 0.35kg

[0074] 9. Deionized water 40.00kg

[0075] The change of each component is mainly adjusted according to the actual demand of different electrical products and the change of common components in order to obtain the best comprehensive performance.

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PUM

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Abstract

The invention discloses a water soluble low-temperature solidification appliance insulating varnish and a preparation method thereof. The water soluble low-temperature solidification appliance insulating varnish comprises a low-temperature latent initiator, wherein the low-temperature latent initiator accounts for 0.10 to 1.5 percent of the total weight of the water soluble low-temperature solidification appliance insulating varnish; and the low-temperature latent initiator is benzoyl peroxide. The preparation method comprises the following steps of: firstly, uniformly mixing acrylic ester, organic silicon resin, polyalcohol, the low-temperature latent initiator and 50 percent de-ionized water with slowly stirring at room temperature; secondly, adding a flatting agent, a curing agent, a defoamer and the other 50 percent de-ionized water in sequence and still stirring slowly; and finally, adding solution of alkylol amine dropwise, and adjusting pH to 8.0 to 9.0 to obtain the required product. When the preparation method is implemented, the baking, solidification and film molding temperature of the varnish is as low as only 80 to 90 DEG C; and a varnish film has high adhesion, high humidity, heat and slat-fog resistance and high water solubility and produces no harmful gas in use.

Description

technical field [0001] The invention relates to an insulating varnish and a preparation method thereof, in particular to a water-soluble low-temperature curing electrical insulation varnish and a preparation method thereof. Background technique [0002] The insulation varnishes widely used in electrical appliances (such as small and medium-sized transformers, coils, micro-motors, etc.) In the process of storage, transportation and use, there are potential safety hazards, which are not conducive to production and endanger the health of users. [0003] The water-soluble insulating varnish is favored by people due to its advantages of environmental protection, non-toxicity and safety. It is an inevitable trend to develop water-soluble insulating varnish. In developed countries such as Europe, Japan, and the United States, the technology of water-soluble insulating varnishes developed earlier and has some applications. Our country is still in its infancy, only in the developm...

Claims

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Application Information

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IPC IPC(8): C09D133/06C09D183/00C09D5/25
Inventor 梁树华邱彩虹王素波余章炼
Owner 深圳市东方亮化学材料有限公司
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