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Magnesium alloy vermiculite pumice ferric oxide composite material and preparation method thereof

A composite material and iron oxide technology, which is applied in the aluminum alloy vermiculite pumice iron oxide composite material and its preparation method and its preparation field, can solve the problems of poor microwave absorption performance and achieve the effect of large electromagnetic wave absorption range

Inactive Publication Date: 2012-08-22
淮安市清河区科技转化服务中心
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage of this material is poor absorbing performance

Method used

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  • Magnesium alloy vermiculite pumice ferric oxide composite material and preparation method thereof
  • Magnesium alloy vermiculite pumice ferric oxide composite material and preparation method thereof
  • Magnesium alloy vermiculite pumice ferric oxide composite material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] The preparation process of the aluminum alloy base vermiculite pumice iron oxide composite material of the present invention is as follows:

[0033] a. Preparation of vermiculite pumice iron oxide compound: first put ferric chloride and ammonium ferrous sulfate into a hydrothermal container with Teflon lining, add water to dissolve (add a small amount of water until dissolved), and then put Vermiculite and pumice, the size of pumice particles is 0.5mm, the size of vermiculite particles is 0.05mm, the weight ratio of vermiculite and pumice is 0.01:1, stir the above materials for 2-7min, ferric chloride, ferrous ammonium sulfate and vermiculite The weight ratio of the stone-pumice mixture is 1:1:1. After the stirring is completed, place the stirred material in an oven at 220° C. for 3 hours and then cool naturally to obtain the vermiculite-pumice-iron oxide compound;

[0034] b. Preparation of titanium fiber: by weight percentage, Cu is 0.003%-0.09%, Sm is 0.003%-0.09%, a...

Embodiment 2

[0039] When preparing the vermiculite pumice iron oxide composite, the weight ratio of vermiculite and pumice is 0.1:1; the weight ratio of ferric chloride, ferrous ammonium sulfate and vermiculite pumice mixture is 1:1:2, and the size of pumice particles is 1mm , the size of vermiculite particles is 0.3mm,

[0040]Preparation of titanium fiber: by weight percentage containing Cu is 0.09%, Sm is 0.03%, and the rest is Ti for batching,

[0041] When the composite preform is prepared, the composite preform is controlled to account for 45% of the cavity volume of the metal mold;

[0042] Preparation of aluminum alloy liquid: each component is proportioned by weight percentage Ti is 0.8%, Th is 0.05%, Si is 1%, and the rest is Al;

[0043] The preparation process is the same as in Example 1.

Embodiment 3

[0045] When preparing the vermiculite pumice iron oxide compound, the weight ratio of vermiculite and pumice is 0.05:1; the weight ratio of ferric chloride, ferrous ammonium sulfate and vermiculite pumice mixture is 1:1:1.5, and the size of pumice particles is 0.7 mm, the size of vermiculite particles is 0.07mm,

[0046] Preparation of titanium fiber: by weight percentage, Cu is 0.003%-0.09%, Sm is 0.003%-0.09%, and the rest is Ti for batching;

[0047] When the composite preform is prepared, the composite preform is controlled to account for 55% of the cavity volume of the metal mold;

[0048] Preparation of the aluminum alloy: each component is 0.5% by weight of Ti, 0.03% of Th, 0.6% of Si, and the rest is Al for batching;

[0049] The preparation process is the same as in Example 1.

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Abstract

The invention provides a magnesium alloy vermiculite pumice ferric oxide composite material and a preparation method thereof. The composite material has high microwave-absorbing performance and excellent damping performance. The preparation method has simple process and low production cost and is suitable for industrialized production. The composite material takes a magnesium alloy as a substrate, a vermiculite pumice ferric oxide compound and titanium fiber are distributed on the substrate, and each compound particle is 0.5-1mm; the vermiculite pumice ferric oxide compound and the titanium fiber are 45-55 percent by volume of the composite material; the magnesium alloy substrate is prepared from the following chemical components in percentage by weight: 0.3-0.8 percent of Ti, 0.01-0.05 percent of Th, 0.5-1 percent of Si and the balance of Al; and the titanium fiber is prepared from the components in percentage by weight: 0.003-0.09 percent of Cu, 0.003-0.09 percent of Sm and the balance of Ti.

Description

1. Technical field [0001] The invention belongs to the field of metal materials, and relates to an aluminum alloy vermiculite pumice iron oxide composite material and a preparation method thereof. 2. Background technology [0002] At present, in the field of materials, the wave-absorbing and vibration-reducing effect of materials has been paid attention to. [0003] CN200410023374.1 relates to an aluminum-based wave-absorbing material and its preparation method, which is characterized in that: the surface layer of an aluminum or aluminum alloy plate is formed by a one-step or two-step anodic oxidation method of direct current or alternating current to form a porous aluminum oxide film to form an aluminum-based porous oxide film Aluminum template, that is, AAO template; use DC or pulse current electrochemical deposition to assemble magnetic nano-metal wire arrays in aluminum-based AAO porous membranes to make aluminum-based absorbing materials for in-situ assembly of magnetic...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C47/08C22C49/06C22C21/00
Inventor 赵浩峰王玲李鹏
Owner 淮安市清河区科技转化服务中心