Method for preparing ultrapure copper ingot
A technology of ultra-pure copper and preparation process, which is applied in the field of preparation of ultra-pure copper ingots, which can solve problems such as the gap between density and theoretical density, difficulty in meeting special user requirements, and difficulty in avoiding pollution of melting crucibles, etc., to achieve diversification , improve product quality, optimize the effect of physical properties
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Embodiment 1
[0022] Manually adjust the process parameters as follows for ultra-pure copper ingot casting:
[0023] Filament voltage
8V
20A
Auxiliary high voltage
1.0kV
bombardment current
1.3A
main high voltage
19kV
electron beam
2.2A
a focusing current
90mA
Two focusing currents
70mA
triple focus current
30mA
Accelerating pole current
54.2mA
A column of hole current
64mA
Two-lane hole current
63mA
[0024] Test and analyze the samples of the ultrapure copper ingots prepared above. 68 non-gas elements were detected and analyzed by GDMS (glow discharge mass spectrometry), and 4 gas contents were detected and analyzed by LECO method. The results are shown in Table 1. The total non-gas impurity content is about 1ppm, and the purity of ultrapure copper ingot reaches 99.9999 %.
[0025] Table 1 Purity analysis results of ultrapure copper ingots
[0026] ...
Embodiment 2
[0029] Manually adjust the process parameters as follows for ultra-pure copper ingot casting:
[0030] Filament voltage
8.6V
24A
Auxiliary high voltage
1.2kV
bombardment current
1.5A
main high voltage
21kV
electron beam
2.4A
a focusing current
100mA
Two focusing currents
74mA
triple focus current
46mA
Accelerating pole current
63.1mA
A column of hole current
72.5mA
Two-lane hole current
70.3mA
[0031] Test and analyze the samples of the ultrapure copper ingots prepared above. 68 non-gas elements were detected and analyzed by GDMS (glow discharge mass spectrometry), and 4 kinds of gas content were detected and analyzed by LECO method. The results are shown in Table 2. The total non-gas impurity content is about 0.8ppm, and the purity of ultra-pure copper ingot reaches 99.99992%.
[0032] Table 2 Purity analysis results of ultrapure copper i...
Embodiment 3
[0036] Manually adjust the process parameters as follows for ultra-pure copper ingot casting:
[0037] Filament voltage
9.3V
28A
Auxiliary high voltage
1.3kV
bombardment current
1.6A
main high voltage
23kV
electron beam
2.4A
a focusing current
110mA
Two focusing currents
77mA
triple focus current
50mA
Accelerating pole current
66.5mA
A column of hole current
83mA
Two-lane hole current
79.4mA
[0038] Test and analyze the samples of the ultrapure copper ingots prepared above. 68 non-gas elements were detected and analyzed by GDMS (glow discharge mass spectrometry), and 4 gas contents were detected and analyzed by LECO method. The results are shown in Table 3. The total non-gas impurity content is about 0.8ppm, and the purity of the ultra-pure copper ingot reaches 0.8 ppm. 99.99992%.
[0039] Table 3 Purity analysis results of ultra-pure copp...
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