Silicone rubber putty and preparation method thereof
A silicone rubber and putty technology, applied in chemical instruments and methods, other chemical processes, filling slurry, etc., can solve the problems of short service life of putty, non-compliance with environmental protection requirements, poor sealing performance, etc., so that it is not easy to weather and easy to remove , the effect of not easy to deform
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[0040] The preparation method of silicone rubber putty of the present invention comprises the steps:
[0041] Step 1: the mass fraction is 70-80% silicone rubber raw rubber (vinyl content is 0.01-0.2%), 0.1-1% boric acid, 0.1-10% AlCl 3 or FeCl 3 , Put 5-30% of inorganic filler into the kneader and stir evenly, heat to 130°C-140°C, knead until the material is drawn, cool to room temperature, add 0.1-10% softener, and neutralize the adsorbent in the Mix well on a double-roller machine to obtain rubber compound A.
[0042] The resulting compound is characterized by its excellent ductility at low shear rates and its natural leveling if placed on a flat surface. But not only that, its biggest characteristic is that its viscosity will increase dramatically with the change of shear rate, showing a non-linear change. When gently stretched by hand, a very long silk thread can be pulled out, similar to the common chewing gum in life. When stretched quickly by hand, it will break, a...
Embodiment 1
[0049] 125kg of raw rubber (vinyl content of 0.08%, weight average molecular weight of 650,000), 1.2kg of AlCl 3 , 1.0 kg of boric acid, 20 kg of fumed silica (Wacker chemical N20) and 0.5 kg of H 2 O was put into a kneader with a volume of 300L and stirred evenly, heated to 135°C and kneaded until drawing, discharged, after cooling, added 1% triglyceride and 2.5kg of MgO and kneaded on a double-roller to obtain a rubber compound A1 .
Embodiment 2
[0051] 125kg of raw rubber (vinyl content of 0.08%, weight average molecular weight of 650,000), 1.0kg of FeCl 3 , 1.0 kg of boric acid, 20 kg of fumed silica (Wacker chemical N20) and 0.5 kg of H 2 O was put into a 300L kneader and stirred evenly, heated to 135°C and kneaded until drawing, discharged, and after cooling, 1% monomolecular glyceride and 2.5kg of MgO were added and kneaded evenly on a double-roller to obtain rubber compound A2.
[0052] Example 1
[0053] Put 260kg of raw rubber (vinyl content of 0.20%, weight average molecular weight of 650,000), 130kg of fumed silica (Wacker chemical N20) and 26kg of hydroxyl silicone oil into a 300L kneader and stir evenly, and heat to 150 ℃, keep 3h, discharge, after cooling, knead on a kneader to get the rubber mix B. Then, the mixed rubber A1 and the mixed rubber B obtained in the relevant example 1 were mixed uniformly on a two-roll kneader at a mass ratio of 3:7, and a silicone rubber putty that would not be structured ...
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