Topical composition for external use and process for producing the same
A topical composition, water-soluble polymer technology, applied in the direction of drug combination, cosmetic preparations, medical preparations containing active ingredients, etc., can solve the problem of difficult to maintain stability, increase surfactant, safety and use experience Deterioration and other problems, to achieve the effect of good dispersion stability
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Embodiment 1-A to 1-F
[0293] (Examples 1-A to 1-F, Comparative Example 1-G)
[0294] The components described in the composition of Oil Phase Liquid 1 below were stirred at room temperature for 1 hour to prepare Oil Phase Liquid 1 .
[0295]
[0296] Ceramide 3 [ceramide compound, embodiment 1-5] 0.1 parts
[0297] Ceramide 6 [ceramide compound, embodiment 1-7] 0.1 parts
[0298] Phytosphingosine 0.07 parts
[0299] Ethanol [water-soluble organic solvent] 150 parts
[0300] 1N hydrochloric acid (adjusted so that the pH becomes 7 or lower immediately after dispersion)
[0301] Using the KM-type micro-mixer 100 / 100 of the collision type, the resulting oil phase liquid 1 (oil phase) and water (water phase) are micro-mixed with a ratio (mass ratio) of 1:7 to obtain emulsion 1 (dispersion Compositions with ceramides).
[0302] The conditions for using the micromixer are as follows:
[0303] -Microchannel-
[0304] Microchannels on the oil phase side
[0305] Cross-sectional phase / width / depth / l...
Embodiment 2-A to 2-F
[0316] (Examples 2-A to 2-F, Comparative Example 2-G)
[0317] The following components were stirred at room temperature for 1 hour to prepare oil phase liquid 2.
[0318] Ceramide 3 [ceramide compound, embodiment 1-5] 0.1 parts
[0319] Ceramide 6 [ceramide compound, embodiment 1-7] 0.1 parts
[0320] Phytosphingosine 0.03 parts
[0321] Ethanol [water-soluble organic solvent] 150 parts
[0322] 1N hydrochloric acid (adjusted so that the pH becomes 7 or lower immediately after dispersion)
[0323] Then, the components described in Table 2 below were stirred at room temperature for 5 hours to prepare additive solutions 2-A to 2-F (unit: part).
[0324] Using a collision-type KM-type micro-mixer 100 / 100, the resulting oil phase liquid 2 (oil phase) and each of the additive liquids 2-A to 2-F as the water phase were mixed in a ratio (mass ratio) of 1:7 Mix slightly to obtain Compositions 2-A to 2-F for External Use.
[0325] External preparation 2-G for comparison was prep...
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