TiN coating silicon carbide fiber reinforced titanium-based composite material and preparation method thereof

A technology of titanium-based composite materials and silicon carbide fibers, which is applied in the field of coated carbon fiber-reinforced titanium-based composite materials and its preparation, can solve problems such as poor interface strength of TiN-coated silicon carbide fiber-reinforced composite materials, and reduce the degree of interface reaction. Achieve good material performance, reduce the degree of interfacial reaction, and good interface performance

Inactive Publication Date: 2012-10-10
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The purpose of the present invention is to provide a TiN-coated silicon carbide fiber-reinforced titanium-based composite material and its preparation method, which can effectively reduce the degree of interfacial reaction, obtain moderate interfacial reaction intensity, and can effectively control the element in the titanium matrix to the fiber. Diffusion-induced poor interfacial strength of TiN-coated SiC fiber-reinforced composites

Method used

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  • TiN coating silicon carbide fiber reinforced titanium-based composite material and preparation method thereof
  • TiN coating silicon carbide fiber reinforced titanium-based composite material and preparation method thereof
  • TiN coating silicon carbide fiber reinforced titanium-based composite material and preparation method thereof

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specific Embodiment approach 1

[0012] Specific Embodiment 1: The TiN-coated silicon carbide fiber-reinforced titanium-based composite material of this embodiment is made by vacuum hot pressing of alternately stacked foils and TiN-coated silicon carbide fiber cloth. The TiN-coated silicon carbide The thickness of the TiN coating on the fiber cloth is 1-3 μm, and the TiN coating is applied to the surface of the silicon carbide fiber by magnetron sputtering technology, and the foil material is titanium foil, titanium alloy foil or titanium aluminum alloy foil.

[0013] The interface reaction degree of the TiN-coated silicon carbide fiber-reinforced titanium-based composite material in this embodiment is significantly reduced, has good interface properties, and has greatly improved tensile strength.

specific Embodiment approach 2

[0014] Embodiment 2: This embodiment differs from Embodiment 1 in that the thickness of the TiN coating of the TiN-coated silicon carbide fiber cloth is 2 μm. Other parameters are the same as in the first embodiment.

specific Embodiment approach 3

[0015] Embodiment 3: This embodiment is different from Embodiment 1 or Embodiment 2 in that the thickness of the foil is 50 μm to 200 μm. Other parameters are the same as those in Embodiment 1 or Embodiment 2.

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Abstract

The invention discloses a TiN coating silicon carbide fiber reinforced titanium-based composite material and a preparation method thereof and relates to preparation methods of a TiN coating, and a coating carbon fiber reinforced titanium-based composite material. The composite material is formed by performing vacuum hot-forming on foil and TiN coating silicon carbide fiber cloth which are alternately stacked. The preparation method comprises the following steps of: coating the TiN coating on the silicon carbide fiber cloth by magnetron sputtering technology; alternately stacking the TiN coating silicon carbide fiber cloth and the foil, and putting in a graphite mould; and performing vacuum hot-forming on the graphite mould in vacuum hot-press equipment. The TiN coating can effectively prevent the extent of the interface reaction between the silicon carbide fiber and a titanium matrix and effectively inhibit the titanium matrix element from diffusing to the fiber; the fiber is not directly reacted with the matrix; and the interfacial debonding force Pmax of the composite material is 23 to 27N and is smaller than that of a coating-free silicon carbide fiber reinforced titanium-basedcomposite material, namely 33 to 37N, and the moderate interface bonding strength is achieved.

Description

technical field [0001] The invention relates to a coated carbon fiber reinforced titanium-based composite material and a preparation method thereof. Background technique [0002] Silicon carbide fibers have good high-temperature performance, high strength, high modulus and chemical stability, and are widely used in high-tech fields such as aerospace, ships, missiles, weapons, and atomic energy. The outstanding advantage of silicon carbide fiber is high temperature resistance, which is the highest working temperature among the reinforced materials currently used. Advanced composite materials prepared with silicon carbide fiber can work at high temperature for a long time. Silicon carbide long fiber reinforced titanium matrix composites have high specific strength and specific stiffness, high service temperature, good fatigue and creep resistance, and obvious weight reduction effect. A new material that will have great application potential in the aerospace field in the futur...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C49/11C22C49/14C22C47/04C22C47/20C22C101/14C22C121/02
Inventor 陈玉勇杜赵新孔凡涛肖树龙徐丽娟
Owner HARBIN INST OF TECH
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