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271 results about "Titanium foil" patented technology

Titanium dioxide nano thread, belt and tube block array and preparation method thereof

The present invention provides a titanium dioxide nanometer thread, strip and tube block array, and a preparation method of the same, which relates to a nanometer material and a preparation method of the same. A high purity titanium foil serves as a substrate; a mixture solution of ethylene glycol and fluorination ammonification with a content of 0.1~0.5 wt%; a titanium dioxide nanometer thread, strip and pipe block array, which has a nanometer thread, strip blended fasciculation substance of 1~20 micron at the upper end and a regular nanometer tube array at the lower part, is formed vertically at the substrate by constant pressure anodisation. The preparation method comprises the steps of that: the substrate serves as the anode, the platinum serves as the cathode, the distance between the anode and the cathode is 10~50 mm, the voltage is 10~60 V, the reaction time is 30~3000 min; the obtained product is roasted for 1~3 hours at 240~600 DEG C, and is cooled in the furnace, thereby the titanium dioxide nanometer thread, strip and tube block array is obtained. The method has a simple equipment, an excellent repetitiveness for technology, a steady quality of product, and can be used for the fields of photocatalysis, photolysis water, solar cell and spinning electron.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS

Method for brazing ceramic and metal by adopting composite high-entropy alloy solder

The invention relates to a method for brazing ceramic and metal by adopting a composite high-entropy alloy solder, and solves the problem of poor joint performance due to that a lot of brittle intermetallic compounds are generated on the joint surface during the ceramic and metal brazing process. The composite high-entropy alloy solder comprises an upper layer and a lower layer, wherein the upper layer is a high-entropy alloy foil band close to one side of the metal, and the lower layer is titanium foil close to one side of the ceramic. The method comprises the following steps: cleaning a substrate to be welded and the solder foil band, assembling a sandwich structure, applying a pressure of 0.01-0.03 MPa on the sandwich structure to ensure that the substrate can be in full contact with the solder layer, and placing the assembled part in a vacuum diffusion furnace for brazing after the completion of assembly. The method for brazing ceramic and metal by adopting the composite high-entropy alloy solder has the benefits as follows: the operation is simple, the high-entropy effect of the high-entropy alloy is utilized, an FCC and BCC solid solution structure is formed in the brazing seam, no brittle intermetallic compound is generated in the joint, that is, the generation of brittle intermetallic compounds in the joint is effectively suppressed, the reaction between active element Ti and ceramic in titanium foil is utilized, and tough compounds are generated on the joint surface so as to realize the effective metallurgical bonding of ceramic and metal.
Owner:BEIJING UNIV OF TECH

Preparation method of Ag2S/TiO2 composite film photo-anode for photoproduction cathode protection

The invention provides a preparation method of an Ag2S/TiO2 composite film photo-anode for photoproduction cathode protection and relates to a composite film anode. The preparation method of the Ag2S/TiO2 composite film photo-anode for photoproduction cathode protection provided by the invention has high efficiency and low toxicity. The preparation method comprises the following steps of: (1) preparing a titanium substrate sample, namely with a titanium foil as a substrate, sequentially carrying out ultrasonic washing on the titanium foil in acetone, absolute ethyl alcohol and deionized water to obtain the titanium substrate sample; (2) preparing a TiO2 nanotube array film on the surface of titanium, namely dissolving NH4F in the ionized water, adding glycerol to uniformly mix, carrying out anode oxidation by using platinum as a counter electrode, calcining the sample, and cooling the sample along with a furnace to room temperature, and therefore, the TiO2 nanotube array film is prepared on the surface of the titanium; and (3) preparing an Ag2s/TiO2 composite film, namely preparing Ag2S nanoparticles on the surface of the TiO2 nanotube array film to prepare the Ag2S/TiO2 composite film photo-anode for photoproduction cathode protection.
Owner:XIAMEN UNIV

Welding method for micro-plasma arc welding of pure titanium foil

The invention discloses a welding method for micro-plasma arc welding of a pure titanium foil, in particular the welding of the pure titanium foil of which the titanium content is over 99 percent and the thickness is of 0.05 mm, and relates to the technical field of welding. The method comprises the following steps of: cutting the pure titanium foil to be welded into required sizes; selecting two pure titanium foils (4) and (7), and removing oil stains at the peripheries of the sides to be welded thereof; assembling the two pure titanium foils between fixtures of a tooling system; lapping the sides to be welded for about 0.1 to 0.2 mm so as to ensure a welding seam on grooves (6) of base plates of the fixtures; driving a welding torch to move along the welding seam (9) above the welding seam by a motor on the tooling system; and adopting a pulse current for welding. The welding method for the micro-plasma arc welding of the pure titanium foil realizes the butt welding of the micro-plasma arc welding of the pure titanium foil of 0.05 mm, solves the problems of the deformation and burning of the welding of the pure titanium, saves welding cost without adding a filling metal in the welding seam, is favorable for industrial popularization, and fills the blank of the micro-plasma arc welding in the field of pure titanium foils.
Owner:SHANGHAI UNIV OF ENG SCI

Preparation method for Ag/SnO2/TiO2 composite membrane photoanode used for photogenerated cathodic protection

The invention relates to preparation methods for an Ag / SnO2 / TiO2 composite membrane photoanode used for photogenerated cathodic protection, and relates to a composite membrane photoanode, and provides a preparation method for the efficient stable Ag / SnO2 / TiO2 composite membrane photoanode used for photogenerated cathodic protection. The preparation method comprises: 1) preparing a titanium substrate sample, specifically taking titanium foil as a substrate, and performing ultrasonic cleaning successively in acetone, absolute ethanol and deionized water to obtain a titanium substrate sample; 2) preparing a titanium-surface TiO2 nanotube array membrane, specifically dissolving NH4 in deionized water, adding glycol, mixing uniformly, taking platinum as a counter electrode, performing anodization, calcining the titanium substrate sample, and cooling to room temperature along the furnace, so as to obtain the TiO2 nanotube array membrane on the surface of titanium; and 3) preparing the Ag / SnO2 / TiO2 composite membrane, specifically preparing Ag and SnO2 nanometer particles on the surface of the TiO2 nanotube array membrane, so as to obtain the Ag / SnO2 / TiO2 photoanode used for photogenerated cathodic protection.
Owner:INST OF OCEANOLOGY - CHINESE ACAD OF SCI

Preparation method of AgCuTi alloy, preparation method of foil strip brazing filler of AgCuTi alloy, and products of AgCuTi alloy

The invention discloses a preparation method of an AgCuTi alloy, a preparation method of a foil strip brazing filler of the AgCuTi alloy, and products of the AgCuTi alloy. The preparation method is used for solving problems in the prior art that segregation of conventional AgCuTi alloy is easily caused, element Ti is combined with oxygen, activity reducing of brazing filler may be caused in sealing, and in full alloying process, microdefects such as easily caused increasing of grain size and holes are difficult to eliminate, Ag-Ti and Cu-Ti brittle phases are formed from Ti element, and Ag and Cu, and high quality foil strips are difficult to form via rolling. According to the preparation method, vacuum presintering of a powder billet at low temperature is carried out, segregation is inhibited, and hot isostatic pressure medium temperature sintering is adopted, so that grain size and oxygen content are controlled effectively, high density alloy with excellent mechanical properties is obtained, and finally foil strip brazing filler is formed via a plurality of times of direct cold rolling. The preparation method is capable of satisfying requirements on high performance silver copper titanium foil strip brazing filler used in dissimilar material component sealing, is promising in application prospect, and is worthy of large scale popularization and application.
Owner:MATERIAL INST OF CHINA ACADEMY OF ENG PHYSICS

Preparation method of zinc-doped titanium dioxide nano-tube array

The invention belongs to the technical field of photoelectric materials and specially, relates to a preparation method of a zinc-doped titanium dioxide nano-tube array. The preparation method comprises the following steps that 1, an electrolyte of a HF aqueous solution having HF content of 0.3 to 1.0 wt%, an anode of pure titanium foil subjected to surface pretreatment and a cathode of a Pt sheet undergo an electrochemical anodization reaction under direct voltage of 10 to 50V to produce a titanium dioxide nano-tube array; and the titanium dioxide nano-tube array as a cathode, an anode of a platinum sheet and an electrolyte of a Zn(NO3) solution having concentration of 0.1 to 0.5mol/L undergo an electrochemical deposition reaction under direct voltage of 0.3 to 1.0V so that zinc is added into titanium dioxide nano-tube layers and the zinc-doped titanium dioxide nano-tube array is obtained. The preparation method provided by the invention has the advantages that ion implantation time is short; and doped ions Zn<2+> can enter into a titanium dioxide nano-tube under a electric field force and capillary action so that the zinc-doped titanium dioxide nano-tube array having good photoelectric properties and a light absorption range widen to a visible light range is prepared.
Owner:CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY

Cold rolling titanium foil process

The invention provides a cold rolling titanium foil process to meet requirements of ultrathin titanium foil machining. The cold rolling titanium foil process is carried out according to the following procedures that (1) blank materials are chosen and processed: hydrogen aluminum blank materials are chosen to be processed in a polished mode; (2) primary rolling is achieved: the blank materials are polished, the materials are reversed, intersected and repeatedly rolled through a multi-roll foil rolling machine for a plurality of times to achieve the fact that the thickness of the materials reaches 0.18mm-0.22mm; (3) end products are rolled: foil materials after primary rolling are rolled to the foil materials with the thickness of 0.05mm-0.003mm, and fatting, cleaning and lapping are achieved; and (4) packaging and annealing are achieved: under the state that titanium foil is naturally relaxed, the titanium foil is packaged through metal zirconium foil good at hydrogen absorption and oxygen absorption, and after the annealing is achieved in a vacuum furnace, the materials out of the furnace are cooled to be in the room temperature to become end products. The prepared foil materials have the advantages of being good in malleability, high in specific strength, excellent in strength of extension and rigidity, and the like.
Owner:宝鸡市星宏昌金属科技有限公司
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