Detection method of concentrated pills for treating hyperplastic disease of breast

A technology of breast hyperplasia and detection method, applied in sexual diseases, measuring devices, pharmaceutical formulations, etc., can solve the problem of lack of anti-uterine fibroids Chinese patent medicine, etc., and achieve the effect of ensuring the quality of finished products

Active Publication Date: 2011-07-13
雷允上药业集团有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, there are mainly Guizhi Fuling pills / capsules, Gongliuxiao capsules, and Dahuang Zhechong pills for the treatment of uterine fibroids, but there is still a lack of Chinese patent medicines with definite anti-uterine fibroids and high safety factor

Method used

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  • Detection method of concentrated pills for treating hyperplastic disease of breast
  • Detection method of concentrated pills for treating hyperplastic disease of breast

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] Embodiment one: the preparation of concentrated pill

[0036] The concentrated pill formula is: Bupleurum 125g, Cyperus cyperi 125g, Rhubarb (wine-roasted) 83.4g, Qingpi 83.4g, Chuanxiong 83.4g, Curcuma 83.4g, Earthworm 83.4g, Fritillaria 83.4g, Angelica 125g, Paeoniae Alba 125g , Wang Buliuxing 83.4g, made into 1000 pills.

[0037] Take 1 / 2 of the prescription amount of rhubarb and grind it into fine powder for later use.

[0038] Add 5 times the amount of 70% ethanol to Fritillaria fritillaria and Wangbuliuxing, reflux extraction twice, 2 hours each time, filter, combine the filtrate, let it stand for 16 hours, filter, recover the ethanol from the filtrate and concentrate it into a clear paste, set aside .

[0039] Cyperus cyperi, green bark, chuanxiong, zedoary and angelica were steam distilled for 6 hours to extract the volatile oil, and the distilled aqueous solution was filtered for later use. The volatile oil was clathrated with β-cyclodextrin, and the clathrat...

Embodiment 2

[0051] Embodiment two: The detection method of the concentrated pill for the treatment of mammary gland hyperplasia comprises the following steps, specifically ：

[0052] a、 Properties: According to the actual state of large-scale production samples, this product is described as a black charcoal-coated concentrated pill with a dark brown core; the smell is fragrant, and the taste is slightly salty and bitter.

[0053] 、 Extraction inspection: Take about 4g of this product under the weight difference item, grind it finely, weigh it accurately, put it in a conical flask, add 100ml of methanol, seal it tightly, weigh it, put it in a water bath for reflux for 1 hour, and place it at room temperature , weigh again, make up the lost weight with methanol, shake well, filter, discard the initial filtrate, accurately measure the subsequent filtrate 50ml, evaporate to dryness, add 5ml of 10% sodium hydroxide solution to the residue to dissolve, and transfer to In the separatory fun...

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Abstract

The invention discloses a detection method of concentrated pills for treating hyperplastic disease of breast, comprising five steps as follows: character examination, identification, routine pill examination, extract examination and content measurement. The formula of the concentrated pills comprises 125g of radix bupleuri, 125g of rhizoma cyperi, 83.4g of rhubarb (baked with wine), 83.4g of pericarpium citri reticulatae viride, 83.4g of ligusticum wallichii, 83.4g of curcuma zedoary, 83.4 g of ground beetle, 83.4g of thunberg fritillary bulb, 125g of Angelica sinensis, 125g of radix paeoniae alba and 83.4g of cowherb seed. The detection method is in favor of ensuring the quality of finished concentrated pills.

Description

technical field [0001] The invention belongs to the technical field of traditional Chinese medicines, and in particular relates to a method for detecting concentrated pills for treating mammary gland hyperplasia. Background technique [0002] Mammary gland hyperplasia is a common women's surgical disease, and its incidence rate is high, which seriously affects the physical and mental health of women. This disease has the risk of developing into breast cancer. Therefore, it is of great significance to actively treat hyperplasia of mammary glands, improve women's health, and reduce the rate of canceration. Modern medicine believes that the occurrence of mammary gland hyperplasia is due to endocrine dysfunction and ovarian dysfunction, resulting in increased estrogen levels or activity enhancement in the body and decreased progesterone levels. For patients with severe breast hyperplasia pain or obvious local nodules and obvious tenderness, hormone therapy and endocrine therapy...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/9066G01N30/02G01N30/90A61P15/14A61K35/64
Inventor 石荣火叶华钱坤陈琴孙玲
Owner 雷允上药业集团有限公司
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