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Rhenium-containing Ni3Al-based single crystal alloy

A technology based on single crystal and alloy, applied in the field of alloy, can solve the problem of alloy oxidation resistance, and achieve the effect of high-temperature lasting strength and plasticity

Inactive Publication Date: 2011-08-03
BEIHANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] in Ni 3 In the Al intermetallic compound-based alloy, the γ′ phase and the γ phase can be simultaneously strengthened by adding Mo element, reference 1: Mackay R.A., Ebert L.J.in Proc.5th int symp on Superallous[C].Now York: AIME, 1984: 135-144, Reference 2: Mackay R.A., Nathal M.V. in Micon 86: Optimization of Processing, properties, and Servive Performance Through Microstructural Control [C]. Philadelphia: ASTM, 1988: 202-210 and Reference 3: Giamei A.F., Pearson D.D., Anton D.L. High Temperature Ordered Intermetallic Alloys [C]. Pittsburgh: MRS, 1985: 293-308 studies have shown that when the Mo content is 14wt%, better high temperature creep performance is obtained, but too much Mo will lead to alloy Decreased antioxidant capacity

Method used

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  • Rhenium-containing Ni3Al-based single crystal alloy
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preparation example Construction

[0031] A kind of rhenium-containing Ni that the present invention proposes 3 Al-based single crystal alloy, the composition of which is 7-8wt% of Al, 8-13% of Mo, 0.0005-3wt% of Re, and the rest is Ni by weight percentage; the Ni containing rhenium 3 The Al-based single crystal alloy may also contain more than one Dy, Y or Hf, and the composition is 0.05-0.5wt% Dy, 0.1-1wt% Y or 0.05-0.5wt% Hf. The content of Re is preferably 0.5-3 wt%, more preferably 1-2 wt%. The rhenium-containing Ni 3 Al-based single crystal alloys include three phase structures of γ′ phase, γ phase and rhenium-containing NiMo phase in the as-cast state. The present invention proposes that the rhenium-containing Ni 3 The Al-based single crystal alloy is prepared by the following preparation method, which specifically includes the following steps:

[0032] The first step: preparing liquid metal cooling medium;

[0033] The liquid metal cooling medium is gallium indium alloy or metal tin. The preparati...

Embodiment 1

[0049] A rhenium-containing Ni 3 The composition of the Al-based single crystal alloy, the weight percentage of each element is: 7.4wt% Al, 13% Mo, 0.5% Re, 0.1wt% Dy, 0.1wt% Y, and the rest is Ni. The rhenium-containing Ni 3 Al-based single crystal alloys include three phase structures of γ′ phase, γ phase and rhenium-containing NiMo phase in the as-cast state.

[0050] The rhenium-containing Ni3 The preparation method of Al-based single crystal alloy mainly comprises the following steps:

[0051] The first step: preparing liquid metal cooling medium;

[0052] The liquid metal cooling medium is gallium indium alloy. The preparation of the gallium-indium alloy: the raw materials high-purity gallium (Ga) and high-purity indium (In), by weight percentage: gallium 10wt%, the rest is indium, weighed, put into a beaker and heated to 80 ° C to make it After the reaction is in a liquid state, pour it into a liquid metal cooling tank as a cooling medium, and use vacuum pump oil to...

Embodiment 2

[0065] A rhenium-containing Ni 3 The composition of the Al-based single crystal alloy, the weight percentage of each element is: 7.5wt% Al, 11% Mo, 1% Re, 0.05wt% Dy, 0.5wt% Y, and the rest is Ni.

[0066] The rhenium-containing Ni 3 The preparation method of Al-based single crystal alloy specifically comprises the following steps:

[0067] The first step: preparing liquid metal cooling medium;

[0068] The liquid metal cooling medium is gallium indium alloy or metal tin. The preparation of the gallium-indium alloy: the raw materials high-purity gallium (Ga) and high-purity indium (In), by weight percentage: gallium 30wt%, the rest is indium, weighed, put into a beaker and heated to 200 ° C to make it After the reaction is in a liquid state, pour it into a liquid metal cooling tank as a cooling medium, and use vacuum pump oil to heat the liquid metal cooling tank to maintain the temperature of the cooling tank at 18°C, so that the gallium-indium alloy remains liquid;

[00...

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Abstract

The invention provides a rhenium-containing Ni3Al-based single crystal alloy, which comprises the following components in percentage by weight: 7 to 8 percent of Al, 8 to 13 percent of Mo, 0.0005 to 3 percent of Re and the balance of Ni; and the rhenium-containing Ni3Al-based single crystal alloy also can contain more than one of 0.05 to 0.5 percent of Dy, 0.1 to 1 percent of Y and 0.05 to 0.5 percent of Hf. In the rhenium-containing Ni3Al-based single crystal alloy, the rhenium element is added into a Ni3Al-based single crystal alloy, so that the rhenium element is subjected to solid solution in a gamma' phase and a gamma phase and forms a rhenium atom cluster in short range order in the gamma phase. At high temperature, the diffusion coefficient of rhenium in the gamma phase and the gamma' phase is small, the diffusion coefficients of other alloy elements such as Al, Mo and the like in the gamma phase and the gamma' phase can be reduced, and the high temperature stability of the alloy is improved.

Description

technical field [0001] The invention belongs to the technical field of alloys, in particular to a rhenium-containing Ni 3 Al-based single crystal alloy. Background technique [0002] At present, in the industrial fields of power, petrochemical, transportation, especially aviation and aerospace, the engine is required to have a higher thrust-to-weight ratio and work efficiency, which requires the engine to have a higher operating temperature. At present, nickel-based single crystal superalloys are usually used, but high melting point metals such as W, Ta, Re, and Ru are added to nickel-based single crystal superalloys to make their density and cost higher. At the same time, due to the current use of Ni-based superalloys The temperature has reached 85% to 90% of its melting point, which is close to its use limit. Therefore, the development space of Ni-based superalloys is limited, and it is difficult to meet the requirements of high-temperature structural materials for future...

Claims

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Application Information

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IPC IPC(8): C22C19/03C30B29/52
Inventor 宫声凯张恒汤林志李树索马岳徐惠彬
Owner BEIHANG UNIV
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