In-situ steam explosion method and device

A steam explosion and in-situ technology, applied in chemical instruments and methods, methods of chemically changing substances by using atmospheric pressure, raw material pretreatment, etc., can solve the unsolved problems of entanglement and knotting of hemp fiber raw materials, and experimental analysis of resource waste , Hygienic level requirements and other issues, to achieve the effect of easy separation and combing process, quantitative and qualitative analysis, and simple recycling

Inactive Publication Date: 2013-11-06
INST OF PROCESS ENG CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of the present invention is to solve the problem that the existing steam explosion technology and equipment can not solve the entanglement and knotting of hemp fiber raw materials when they are discharged, the difficulty and loss of raw material recovery, and the heat caused by the high hygiene level requirements of some raw materials and the direct discharge of steam to the atmosphere. Waste, environmental pollution, waste of resources, and troubles to experimental analysis, etc., provide a set of in-situ steam explosion technology and equipment for raw materials, by preparing special-sized material trucks and setting wire mesh to intercept the steam outlet , at the moment of blasting, only the gas is allowed to escape, while the solid material remains in the feed car, which avoids the entanglement problem caused by the movement of raw materials, and can also reduce the loss of raw materials and improve the safety and sanitation factor. The gas enters the gas recovery system, which can be used for qualitative and quantitative analysis and also facilitates the secondary utilization of energy

Method used

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  • In-situ steam explosion method and device

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] The volume of the pressure maintaining tank is 5L, the length is 28.5cm, and the side diameter is 15cm. The steam generator is 15L. The power of the steam generator has been turned on before feeding to obtain saturated water vapor at 220°C. The volume of the buffer tank is 20L, and the area of ​​the coil heat exchanger is 0.1m 2 .

[0016] Take by weighing 200g of hemp bast fiber (average length is about 2m), soak it, after soaking for 1h, stack it in the box-type feeder 5, through the valve 2, push the feeder into the pressure maintenance tank 9, close the valve 1. Open the steam valve 1, feed a certain amount of steam, keep the pressure in the tank 9 at 0.7 MPa for 4 minutes, close the steam valve 1, quickly open the valve 11, the steam enters the pressure maintenance tank and then enters the condensation system 14, collects the condensed liquid, Open the discharge valve 6 again, drag out the cage feeder 5, and obtain the steam-exploded hemp fiber. Observe that the...

Embodiment 2

[0018] The volume of the pressure maintaining tank is 2L, the length is 25cm, and the side diameter is 10cm. The steam generator is 15L. The power of the steam generator has been turned on before feeding to obtain saturated water vapor at 220°C. The volume of the buffer tank is 15L, and the area of ​​the coil heat exchanger is 0.05m 2 .

[0019] Cut the outdoor air-dried corn stalks into 1-2cm blocks (wherein the water content is 14%), weigh 100g (wet weight), add 32g of water to make the water content 35%, after the water is evenly absorbed, add to Inside the box-type feeding truck 5, the feeding truck is pushed into the pressure maintenance tank 9 through the valve 2, and the valve 1 is closed. Open the steam valve 1, feed a certain amount of steam, keep the pressure in the tank 9 at 1.2 MPa for 8 minutes, close the steam valve 1, quickly open the valve 11, the steam enters the pressure maintenance tank and then enters the condensation system 14, collects the condensed liqu...

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Abstract

The invention relates to an in-situ steam explosion method, which is characterized in that the raw materials are subjected to explosion in a steam explosion reactor, then the escaped gas is fed into a gas condensation and recycling system and the remaining materials are kept in situ in the steam explosion reactor. The in-situ steam explosion device comprises a horizontal cylindrical tank; the upper wall of the tank is provided with a pressure gauge, a thermometer and a steam inlet, and the lower wall of the tank is provided with a steam outlet; two ball valves respectively arranged at the two sides of the tank are respectively used as a charging-car inlet and a charging-car outlet; and in the box-type or cage-type reticular charging car with wheels, a steel-mesh plate is arranged in front of a pneumatic ball valve of a steam outlet pipeline, the rear part of the steam outlet pipeline is connected with a buffer vessel and a gas condensation and recycling system, and the bottom of the inside of the buffer vessel is provided with an axial fixed orbit which facilitates the getting-in-and-out of the charging car. By using the device disclosed by the invention, the problems that the winding and knotting of fibrilia materials in the process of discharging, the difficulties and loss in raw material recycling, and the heat waste, environmental pollution, wasting of resources and troubles brought to experimental analysis which are caused by directly emitting the steam to the atmosphere and can not be solved by using the existing steam explosion technology and equipment are solved effectively.

Description

technical field [0001] The invention relates to a material pretreatment method and device thereof, in particular to a material in-situ steam explosion method and equipment. Background technique [0002] Steam explosion pretreatment is a pretreatment method developed in recent years. The raw material is heated to 180-235°C with steam, and the pressure is maintained for a certain period of time. When the sudden decompression is sprayed, the liquid water flashes rapidly, generating a large amount of steam, and the volume of the raw material tissue or cell increases sharply. Destruction; In addition, in the pressure maintenance process, there is also the self-catalysis of the raw material itself, and its main components are partially degraded. [0003] The steam explosion technology first started in 1926, when it was produced intermittently, mainly for the production of man-made fiberboard. Beginning in the 1970s, the technology has also been widely used in the production of a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J3/00D21B1/02
Inventor 陈洪章张玉针
Owner INST OF PROCESS ENG CHINESE ACAD OF SCI
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