Preparation method of YBa2Cu3O7-x(YBCO) high-temperature superconductive thick film
A high-temperature superconducting and thick-film technology, which is applied in the field of preparing a single-layer yttrium-barium-copper-oxygen high-temperature superconducting thick film, can solve problems such as the inability to evaluate superconducting properties, achieve an increase in critical current density, increase current-carrying capacity, and broaden applications range effect
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Embodiment 1
[0026] (1) Weigh yttrium acetate, barium acetate and copper acetate to be 0.005mol, 0.01mol and 0.015mol respectively, mix the yttrium acetate, barium acetate and copper acetate and dissolve them in 100ml deionized water containing 10mol% trifluoroacetic acid to prepare into solution;
[0027] (2) After the solution prepared in step (1) was stirred by a magnetic stirrer for 1 hour, the solvent was evaporated by a rotary evaporator to obtain a gel;
[0028] (3) Add 50ml of methanol to the gel, stir it with a magnetic stirrer for 0.5 hours, and then use a rotary evaporator to evaporate the solvent to further remove impurities such as water to obtain a very pure gel;
[0029] (4) The gel prepared in step (4) is added to the mixed solution of 10ml methanol and 10ml terpineol, the volume ratio of the methanol and terpineol is 1: 1 to make Y, Ba and Cu A solution in which the total ion concentration of the three metals is 1.5 mol / L. The obtained methanol and terpineol solution con...
Embodiment 2
[0035] (1) Weigh yttrium acetate, barium acetate and copper acetate to be 0.01mol, 0.02mol and 0.03mol respectively, mix the yttrium acetate, barium acetate and copper acetate and dissolve in 200ml deionized water containing 20mol% trifluoroacetic acid to prepare into solution;
[0036] (2) After the solution prepared in step (1) was stirred by a magnetic stirrer for 2 hours, the solvent was evaporated by a rotary evaporator to obtain a gel;
[0037] (3) Add 50 ml of methanol to the gel prepared in step (2), stir it with a magnetic stirrer for 1 hour, and then use a rotary evaporator to remove the solvent to further remove impurities such as water to obtain a very pure gel;
[0038] (4) the gel that step (3) makes is added in the mixed liquor of 15ml methanol and 15ml terpineol, and the volume ratio of described methanol and terpineol is 1: 1, makes Y, Ba and Cu A solution in which the total ion concentration of the three metals is 2.0 mol / L. The obtained methanol and terpin...
Embodiment 3
[0044] (1) Weigh yttrium acetate, barium acetate and copper acetate to be 0.015mol, 0.03mol and 0.045mol respectively, mix the yttrium acetate, barium acetate and copper acetate and dissolve them in 300ml deionized water containing 30mol% trifluoroacetic acid to prepare into solution;
[0045] (2) After the solution prepared in step (1) was stirred by a magnetic stirrer for 3 hours, the solvent was evaporated by a rotary evaporator to obtain a gel;
[0046] (3) Add 50 ml of methanol to the gel prepared in step (2), stir it with a magnetic stirrer for 1.5 hours, and then use a rotary evaporator to remove the solvent to further remove impurities such as water to obtain a very pure gel;
[0047] (4) the gel that step (3) makes is added in the mixed liquor of 15ml methanol and 15ml terpineol, and the volume ratio of described methanol and terpineol is 1: 1, makes Y, Ba and Cu A solution with a concentration of three metal ions of 3.0 mol / L. The obtained methanol and terpineol so...
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