Nickel-copper-zinc ferrite material with high surface resistance for panel display
A nickel-copper-zinc ferrite, flat-panel display technology, applied in the direction of inorganic material magnetism, etc., can solve the problem of high surface resistance of inverter magnetic core materials, and achieve the effect of low cost and simple process
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Embodiment 1
[0020] (1) Ingredients: Fe with a purity of 99.5% was weighed respectively 2 o 3 , NiO with a purity of 99.8%, ZnO with a purity of 99.8% and CuO with a purity of 99.7%, the molar ratio of the four is 49.00:18.05:28.10:4.85;
[0021] (2) Primary ball milling: put the powder into a ball mill jar according to the mass ratio of ball:material:water=2:1:1, and then wet mill in a ball mill. The ball milling time is 35 minutes, and the rotation speed is 400r / min;
[0022] (3) Pre-burning: put the ball-milled powder into a resistance furnace for pre-burning, the pre-burning temperature is 900°C, and the holding time is 1 hour;
[0023] (4) Secondary ball milling and mixing of auxiliary components: weigh the pre-burned powder (100% by mass) and auxiliary components: chemically pure TiO 2 (0.01wt%), SnO 2 (0.04wt%), V 2 o 5 (0.01wt%), ZrO 2 (0.1wt%), SiO 2 (0.01wt%), CaO (0.04wt%) and MnO 2 (0.1wt%) is put into ball mill jar, and the mass percent of secondary component is the m...
Embodiment 2
[0028] (1) Ingredients: Fe with a purity of 99.6% was weighed respectively 2 o 3, NiO with a purity of 99.7%, ZnO with a purity of 99.8% and CuO with a purity of 99.8%, the molar ratio of the four is 49.50:17.75:27.85:4.90;
[0029] (2) Primary ball milling: the main components are loaded into a ball mill jar according to the mass ratio of ball:material:water=2:1:1, and then wet milled in a ball mill. The ball milling time is 30 minutes, and the rotation speed is 500r / min;
[0030] (3) Pre-burning: put the ball-milled powder into a resistance furnace for pre-burning, the pre-burning temperature is 800°C, and the holding time is 4h;
[0031] (4) Secondary ball milling and mixing of auxiliary components: weigh the pre-burned powder (according to 100%) and auxiliary components: chemically pure TiO 2 (0.03wt%), SnO 2 (0.02wt%), V 2 o 5 (0.04wt%), ZrO 2 (0.4wt%), SiO 2 (0.02wt%), CaO (0.02wt%) and MnO 2 (0.35wt%) is put into ball mill jar, and the mass percent of secondary...
Embodiment 3
[0036] (1) Ingredients: Fe with a purity of 99.3% was weighed respectively 2 o 3 , NiO with a purity of 99.6%, ZnO with a purity of 99.7% and CuO with a purity of 99.8%, the molar ratio of the four is 50.00:17.55:27.50:4.95;
[0037] (2) Primary ball milling: put the powder into a ball mill jar according to the mass ratio of ball:material:water=2:1:1, and then wet mill in a ball mill. The ball milling time is 40 minutes, and the rotation speed is 600r / min;
[0038] (3) Pre-burning: Put the ball-milled powder into a resistance furnace for pre-burning, the pre-burning temperature is 850°C, and the holding time is 3h;
[0039] (4) Secondary ball milling and mixing of auxiliary components: weigh the pre-burned powder (according to 100%) and auxiliary components: chemically pure TiO 2 (0.02wt%), SnO 2 (0.01wt%), V 2 o 5 (0.03wt%), ZrO 2 (0.5wt%), SiO 2 (0.03wt%), CaO (0.01wt%) and MnO 2 (0.65wt%) is put into ball mill jar, and the mass percent of minor component is the mas...
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