Metal ceramic seal ring material and preparation method thereof
A technology of cermets and sealing rings, which is applied in the field of powder metallurgy and cermets, can solve the problems of adverse effects on corrosion resistance, expensive additives, high brittleness, etc., to improve mechanical properties, avoid the formation of brittle phases, and achieve low density. Effect
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[0012] Example 1: Weigh the raw materials to prepare molybdenum-free cermets, with a particle size of 1.3μm (W,Cr)C accounting for 5%, a particle size of 2.5μm (W,Ti)C accounting for 10%, and a particle size of 1.5μm Ni accounts for 10%, Co with a particle size of 1.2μm accounts for 6%, and the rest is Ti(C,N) with a particle size of 1.8μm. The C:N atomic ratio in Ti(C,N) powder is 7:3, (W The weight ratio of W:Cr in ,Cr)C powder is 98:2, and the weight ratio of WC:TiC in (W,Ti)C powder is 7:3. In the process of ball milling, first add (W,Cr)C and (W,Ti)C powder to the ball mill, add oleic acid and PEG6000 forming agent, and ball mill for 24h; then add Ni, Co, Ti(C,N) powder Ball milling for 36 hours, the ball milling medium is anhydrous ethanol, the addition amount is 280ml, the addition amount of PEG6000 forming agent is 2wt%, the addition amount of oleic acid is 1wt%, the ball milling speed is 65r / min, and the grinding ball is WC- with Φ6mm. 6wt% Ni cemented carbide balls, ...
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[0013] Example 2: Weigh the raw materials to prepare molybdenum-free cermets, with a particle size of 0.8μm (W,Cr)C accounting for 6%, a particle size of 2.0μm (W,Ti)C accounting for 15%, and a particle size of 1.6μm Ni accounts for 8%, Co with a particle size of 1.2μm accounts for 15%, and the rest is Ti(C,N) with a particle size of 1.9μm. The C:N atomic ratio in Ti(C,N) powder is 7:3, (W The weight ratio of W:Cr in ,Cr)C powder is 99:1, and the weight ratio of WC:TiC in (W,Ti)C powder is 7:3. In the ball milling process, first add (W,Cr)C and (W,Ti)C powders to the ball mill, add oleic acid and PEG6000 forming agent, and ball mill for 16h; then add Ni, Co, Ti(C,N) powders Ball mill again for 48 hours, the ball milling medium is anhydrous ethanol, the addition amount is 450ml, the addition amount of PEG6000 forming agent is 5wt%, the addition amount of oleic acid is 0.5wt%, the ball milling speed is 80r / min, and the grinding ball is Φ6mm WC -6wt%Ni cemented carbide balls, the...
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