A kind of method adopting normal pressure method to synthesize zinc cyanurate
A technology of zinc cyanurate and cyanuric acid, which is applied in the direction of organic chemistry, can solve the problems of complicated operation and high cost, and achieve the effect of low reaction temperature, easy control and easy operation
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Embodiment 1
[0014] First, weigh 100kg of cyanuric acid and add it to the reaction kettle, add 100kg of water, turn on the stirring paddle for stirring, set the temperature to 80°C, after the temperature reaches the set temperature, add 94kg of zinc oxide, continue to stir for 1 hour, then open the outlet valve, continue Stir until the mass is dry. Open the discharge port, release the material, put the material into the mechanical pulverizer and jet pulverizer for pulverization and classification.
Embodiment 2
[0016] First, weigh 100kg of cyanuric acid and 85kg of zinc oxide, first add cyanuric acid into the reaction kettle, add 80kg of water, turn on the stirring paddle for stirring, set the temperature at 50°C, and add zinc oxide after the temperature reaches the set temperature, and continue stirring 1.5h, then open the outlet valve and continue stirring until the material is dry. Open the discharge port, release the material, put the material into the mechanical pulverizer and jet pulverizer for pulverization and classification.
Embodiment 3
[0018] First, weigh 100kg of cyanuric acid and 75kg of zinc oxide, first add cyanuric acid into the reaction kettle, add 52.5kg of water, turn on the stirring paddle for stirring, set the temperature at 120°C, and add 75kg of zinc oxide after the temperature reaches the set temperature, Continue stirring for 2 hours, then open the outlet valve, and continue stirring until the material is dry. Open the discharge port, release the material, put the material into the mechanical pulverizer and jet pulverizer for pulverization and classification.
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