Textile composite antibacterial agent and preparation method thereof
A technology for compounding antibacterial agents and textiles is applied in the field of preparation of antibacterial agents to achieve good killing effect.
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Embodiment 1
[0028] The preparation of textile compound antibacterial agent of the present invention:
[0029] Step 1: Wash the soybeans, add 3 times the weight of pure water, soak them at 40°C for 24 hours, peel them, and then use a crushing device to crush them into a slurry;
[0030] Step 2: filter the above muddy substance with 80 mesh filter cloth to obtain white emulsion;
[0031] Step 3: Add 4 times the volume of pure water to the white emulsion, then add 800mg / L chitosan (average molecular weight 7.3×10 5 Da, deacetylation degree 87%) for flocculation, after filtration and separation, a transparent liquid was obtained;
[0032] Step 4: After diluting the above transparent liquid (soybean extract) 50 times, add 1% N-dodecyl-β-alanine sodium, 1% Tween-80, 0.5 % methyl acrylate polymer (molecular weight is 2580Da), 0.4% 3-(trisilanol) propyl dimethyl octadecyl ammonium chloride, the balance is water, and the textile composite antibacterial compound of the present invention can be o...
Embodiment 2
[0035] The preparation of textile compound antibacterial agent of the present invention:
[0036] Step 1: Wash the soybeans, add 2 times the weight of pure water, soak them at 30°C for 48 hours, peel them, and then use a crushing device to crush them into a slurry;
[0037] Step 2: filter the above-mentioned muddy substance with a 60-mesh filter cloth to obtain a white emulsion;
[0038] Step 3: Add 5 times the volume of pure water to the white emulsion, then add 1500mg / L chitosan for flocculation, filter and separate to obtain a transparent liquid;
[0039] Step 4: After diluting the above transparent liquid (soybean extract) 40 times, add 2% N-dodecyl-β-alanine sodium, 2.5% Tween-80, 2 % methyl acrylate polymer (molecular weight is 2580Da), 0.1% 3-(trisilanol) propyl dimethyl octadecyl ammonium chloride, after completely dissolving, obtain the composite antimicrobial agent for textiles of the present invention.
[0040]
Embodiment 3
[0042] The preparation of textile compound antibacterial agent of the present invention:
[0043] Step 1: Wash the soybeans, add 3 times the weight of pure water, soak them at 60°C for 12 hours, peel them, and then use a crushing device to crush them into a slurry;
[0044] Step 2: filter the above-mentioned muddy substance with a 160-mesh filter cloth to obtain a white emulsion;
[0045] Step 3: Add 6 times the volume of pure water to the white emulsion, then add 1000mg / L chitosan (average molecular weight 7.3×10 5 Da, deacetylation degree 87%) for flocculation, after filtration and separation, a transparent liquid was obtained;
[0046] Step 4: After diluting the above transparent liquid (soybean extract) 50 times, add 0.05% N-dodecyl-β-alanine sodium, 0.5% Tween-80, 0.5 % methyl acrylate polymer (molecular weight is 2580Da), 4% 3-(trisilanol) propyl dimethyl octadecyl ammonium chloride, promptly obtain textile compound antibacterial agent of the present invention after dis...
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Abstract
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