Unlock instant, AI-driven research and patent intelligence for your innovation.

Printable etching paste for etching low-emissivity thin film as well as etching method and product thereof

An etching paste and low-radiation technology, which is applied in the field of etching coated glass and coated glass processing, can solve the problems of poor side etching effect, long etching time, and insufficient resistance of 1.0mm line width, so as to achieve good etching effect and raw material Simple, low-cost effect

Active Publication Date: 2013-07-03
FUYAO GLASS IND GROUP CO LTD
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] The technical problem to be solved by the present invention is to apply the existing etching paste to the low-emissivity film. Under the same conditions, the etching time is long, the side etching effect is not good, and the etched 1.0mm line width resistance cannot reach the megohm level. , provide a printable etching paste for etching low-emissivity film, also provide a method for etching low-emissivity glass by using the etching paste, and further obtained etching products

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Printable etching paste for etching low-emissivity thin film as well as etching method and product thereof
  • Printable etching paste for etching low-emissivity thin film as well as etching method and product thereof
  • Printable etching paste for etching low-emissivity thin film as well as etching method and product thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] Etching paste composition:

[0038] 20ml phosphoric acid (85%)

[0039] 3ml iodine (medical use)

[0040] 12g SiO 2 pink

[0041] 3ml deionized water

[0042] While stirring, add phosphoric acid, deionized water, and iodine into the beaker one after another, stir evenly, and then add SiO 2 powder, and stirred for 2h until a uniform etching medium was formed.

[0043] Using a 300-mesh screen with a line width of 1.0 mm, an etching paste was printed on the low-e glass of Example 1 described in Chinese Patent Application No. CN200910054331.2, which can be baked and bent, by screen printing. After printing, put the Low-e glass in an oven, and bake the film layer printed with etching paste at 250°C for 25 minutes. After the baking treatment, use water or weak alkaline water to clean the etching paste on the film layer; use ultrasonic, spray and other methods to achieve better cleaning effect. Finally, bake the etched Low-e glass to remove water marks on the film surfa...

Embodiment 2

[0046] Etching paste composition

[0047] 7ml sulfuric acid (30%)

[0048] 3ml iodine (medical use)

[0049] 6g SiO 2 pink

[0050] 5ml deionized water

[0051] While stirring, add sulfuric acid, iodine, and deionized water to the beaker one after another, stir evenly, and then add SiO 2 powder, and stirred for 2h until a uniform etching medium was formed.

[0052] Using a 300-mesh screen with a line width of 1.0mm, the etching paste was printed on the commercially available Fuyao Low-e glass by screen printing. After printing, put the Low-e glass in an oven, and bake the film layer printed with etching paste at 200°C for 20 minutes. After the baking treatment, use water or weak alkaline water to clean the etching paste on the film layer; use ultrasonic, spray and other methods to achieve better cleaning effect. Finally, bake the etched Low-e glass to remove water marks on the film surface.

[0053] Use a multimeter to test the resistance of the line width is greater t...

Embodiment 3

[0054] Embodiment 3 (comparative example 1)

[0055] Take the commercially available water-based environmental protection etching paste as an example (with acid as the main etching component)

[0056] Using a 300-mesh screen with a line width of 1.0 mm, an etching paste was printed on the low-e glass of Example 1 described in Chinese Patent Application No. CN200910054331.2, which can be baked and bent, by screen printing. After printing, put the Low-e glass into the oven to bake it. After the baking treatment, use water or weak alkaline water to clean the etching paste on the film layer; use ultrasonic, spray and other methods to achieve better cleaning effect. Finally, bake the etched Low-e glass to remove water marks on the film surface.

[0057] The resistance test results are shown in Table 1.

[0058] Table 1 Etching effect table of commercially available water-based environmental protection etching paste

[0059] Etching temperature

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
electrical resistanceaaaaaaaaaa
widthaaaaaaaaaa
Login to View More

Abstract

The invention provides a printable etching paste for etching a low-emissivity thin film as well as an etching method and product thereof, relating to the field of coated glass processing. The etching paste comprises an acidic etching agent, inorganic particles, iodine alcohol solution and unessential additive, and can be printed on low-emissivity thin film glass by silk screen printing, template printing, ink-jet printing and other printing techniques to form patterned low-emissivity coated glass. The etching paste, etching method and product have the advantages that: the etching paste capable of completely etching low-emissivity film layers, in particular an automobile front shield low-emissivity film layer, can be prepared by adopting fewer components, the raw materials are simple, the cost is lower, and the etching paste has good etching effect; and by virtue of the etching paste, a fine structure can be selectively etched on a low-e (low-emissivity) film without or with less damage or erosion to adjacent regions, the etching time is short, the etching speed is high, and the etching temperature is low, thus the resistance at both sides of an etched 1.0mm-wide line reaches the MOmega level and can be greater than 20 M Omega.

Description

【Technical field】 [0001] The invention relates to the field of coated glass processing, in particular to the field of etching coated glass. 【Background technique】 [0002] Low-e glass, also known as Low-e glass, is a film product composed of multiple layers of metal or other compounds coated on the glass surface. Due to its high transmission of visible light and high reflection of mid- and far-infrared rays, low-e glass is a It is an energy-saving and environment-friendly product, which is widely used. [0003] According to the manufacturing process of Low-e coated glass, it can be divided into online Low-e coated glass and off-line Low-e coated glass. The invention belongs to the field of off-line Low-e coated glass. Off-line Low-e coated glass is produced by magnetron sputtering coating technology, and its main functional layer is silver layer. Since the silver layer is particularly easy to oxidize, ordinary off-line Low-e coated glass cannot be heated and can only be use...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C03C15/00
Inventor 何立山福原康太袁军林
Owner FUYAO GLASS IND GROUP CO LTD