Membrane catalytic reactor

A technology of reactor and membrane catalysis, which is applied in chemical instruments and methods, chemical/physical processes, petroleum industry, etc., can solve the problems of difficult recycling of catalyst inorganic alkali, high price of immobilized enzyme, increased reaction cost, etc., and achieves manufacturing The process is simple, the concentration is the same, and the effect of expanding the production scale

Active Publication Date: 2012-06-20
SHANDONG UNIV OF TECH
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

Patent 200810059776.5 prepared an immobilized enzyme membrane reactor and used it to produce biodiesel, which has high production efficiency, but the high price of immobilized enzyme greatly increases the reaction cost
Patent 200910030047.1 invented a method for preparing biodiesel through porous ceramic membrane dispersion and enhanced transesterification reaction. The reaction time is short and the yield is high. However, the catalyst inorganic base used in this method is difficult to recycle and has great corrosion on equipment

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Embodiment Construction

[0021] Further illustrate the present invention below in conjunction with accompanying drawing.

[0022] Such as figure 1 As shown, the present invention comprises feed inlet 6, feed outlet 14, raw material chamber 7, product chamber 13, jacket 4, electric stirrer 1 and catalytic membrane 12, and electric stirrer 1 is arranged on raw material chamber 7 tops, stirring paddle 8 enters the inside of the raw material chamber 7, the catalytic membrane 12 is arranged between the raw material chamber 7 and the product chamber 13, the feed inlet 6 is arranged at the top of the raw material chamber 7, the discharge port 14 is arranged at the bottom of the product chamber 13, and the jacket 4 is arranged at the bottom of the product chamber 13. The outside of the raw material chamber 7 , the catalytic membrane 12 and the product chamber 13 . The catalytic membrane 12 is sheet-shaped and supported by the catalytic membrane support plate 11 . The catalytic membrane 12 and the catalytic ...

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Abstract

The invention belongs to chemical equipment, and particularly relates to a membrane catalytic reactor. The membrane catalytic reactor comprises a feed port, a discharge port, a raw material chamber, a product chamber, a jacket, an electric stirrer and a catalytic membrane, wherein the electric stirrer is arranged above the raw material chamber; stirring paddles extend into the raw material chamber; the catalytic membrane is arranged between the raw material chamber and the product chamber; the feed port is formed on the top of the raw material chamber; the discharge port is formed at the bottom of the product chamber; and the jacket is arranged outside the raw material chamber, the catalytic membrane and the product chamber. By adopting the membrane catalytic reactor for performing esterification reaction, the energy consumption is low, and the reaction efficiency is high; the problems of separation and recovery of a catalyst are avoided, and the product cost is reduced; strongly acidic cation exchange resin powder is used as a catalytically active matter; polyethersulfone is used as a base material; a hybrid membrane which is prepared by a phase conversion method is a catalytic membrane which has higher efficiency for catalytic esterification reaction and has no problems of equipment corrosion, environment pollution and the like; and the membrane catalytic reactor has the advantages of simple equipment structure, high adaptability, easiness in control of process, convenience in operation and suitability for industrial implementation.

Description

technical field [0001] The invention belongs to chemical equipment, in particular to a membrane catalytic reactor. Background technique [0002] Monoalkyl esters of long-chain fatty acids (usually methyl esters, ethyl esters, etc.) obtained by transesterification with short-chain fatty alcohols using animal and vegetable oils and fats as raw materials. The viscosity is close to that of diesel oil, and its performance is similar to that of petroleum diesel. , namely biodiesel. Biodiesel is renewable, environmentally friendly, safe to use and store, non-toxic, does not need to change the existing diesel engine, can partially or completely replace mineral diesel, and is a degradable clean energy. [0003] In China, non-edible oils and waste animal and vegetable oils are the raw materials for the production of biodiesel, such as tung oil, jatropha oil, waste cooking oil, gutter oil, soapstock and acidified oil, etc. Acidified oil refers to the oil obtained by acidifying the by...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/00C10G3/00
CPCY02P30/20
Inventor 丁金城卢杰
Owner SHANDONG UNIV OF TECH
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