Olive oil microcapsule and preparation method thereof
A technology of olive oil and microcapsules, which is applied in the agricultural field, can solve the problems of high price, limited production of natural vegetable gum, and bleak application prospects, and achieve the effects of cheap price, good microencapsulation effect, and superior emulsification and film-forming properties
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Embodiment 1
[0025] Mix 32g of waxy cornstarch with 368g of deionized water, stir evenly to dissolve all the starch, then put it in a 90°C water bath for 1 hour, and stir at a speed of 300r / min. The starch solution after the water bath was subjected to high-speed shearing, pre-shearing at 8000r / min for 2min, and then high-speed shearing at 12000r / min for 4min. The sheared starch solution was passed through a high-pressure homogenizer under a pressure of 40 MPa for one cycle.
[0026] Add 48g of octenyl succinic acid starch ester HI-CAP100 (the degree of esterification is 0.104) to the reaction system, put the mixed solution in a 65°C water bath for 0.5 hours and stir at a speed of 300r / min.
[0027] Add 32g of olive oil. The mixture was placed in a water bath at 65°C for 0.5 hour and stirred at a speed of 300 r / min.
[0028] The solution after the water bath was subjected to high shear, pre-sheared at 8000r / min for 2min, and then high-speed sheared at 12000r / min for 4min. The sheared so...
Embodiment 2
[0032] Mix 28g of waxy cornstarch with 372g of deionized water, stir evenly to dissolve all the starch, then put it in a 90°C water bath for 1 hour, and stir at a speed of 300r / min. The starch solution after the water bath was subjected to high shear, pre-sheared at 8000r / min for 2min, and then high-speed sheared at 12000r / min for 4min. The sheared starch solution was passed through a high-pressure homogenizer under a pressure of 40 MPa for one cycle.
[0033] Add 28g of octenyl succinic acid starch ester HI-CAP100 (the degree of esterification is 0.104) to the reaction system, put the mixed solution in a 65°C water bath for 0.5 hours and stir at a speed of 300r / min.
[0034] Add 16.8g of olive oil. The mixture was placed in a water bath at 65°C for 0.5 hour and stirred at a speed of 300 r / min.
[0035] The solution after the water bath was subjected to high shear, pre-sheared at 8000r / min for 2min, and then high-speed sheared at 12000r / min for 4min. The sheared solution wa...
Embodiment 3
[0039] Mix 20g of waxy cornstarch with 380g of deionized water, stir evenly to dissolve all the starch, then put it in a water bath at 95°C for 1 hour, and stir at a speed of 300r / min. The starch solution after the water bath was subjected to high-speed shearing, pre-shearing at 6000r / min for 2min, and then high-speed shearing at 11000r / min for 4min. The sheared starch solution was passed through a high-pressure homogenizer under a pressure of 30 MPa for one cycle.
[0040] Add 46g of octenyl succinic acid starch ester HI-CAP100 (the degree of esterification is 0.104) to the reaction system, put the mixed solution in a 65°C water bath for 0.5 hours and stir at a speed of 300r / min.
[0041]Add 13.2g of olive oil. The mixture was placed in a water bath at 65°C for 0.5 hour and stirred at a speed of 300 r / min.
[0042] The solution after the water bath was subjected to high shear, pre-sheared at 6000r / min for 2min, and then high-speed sheared at 11000r / min for 4min. The sheare...
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