755 results about "Starch solution" patented technology

The invention belongs to the technical field of natural polymer modification and discloses a preparation method of a starch and fatty acid compound. The method comprises the following steps: adding de-ionized water into starch and balancing moisture in a closed container; carrying out heat treatment to obtain the starch subjected to wet and hot treatment; then adding a buffering solution to prepare a starch solution; after pre-heating, adding 2 to 5u/g pullulanase liquid to react for 4 to 5 hours; after carrying out enzyme deactivation, centrifuging and separating to obtain enzyme treatment modified starch; then stirring and gelatinizing the starch in a boiled water bath for 25 to 45 minutes and cooling to 60 to 90 DEG C to obtain gelatinized starch; then transferring the gelatinized starch into a homogenizing machine and adding fatty acid to carry out homogenization and mixing; and keeping the heat of the water bath to synthesize for 30 to 40 minutes to obtain the starch and fatty acid compound. According to the preparation method, a greener and more environment-friendly new way is provided for synthesizing the starch and fatty acid compound through wet and hot treatment and controlled enzymolysis treatment by adopting a gelatinizing method.

The invention discloses a preparation method of a regenerated cellulose reinforced starch film. The method comprises the steps of dissolving cellulose by taking an alkaline/urea mixed water solution or alkaline/thiourea mixed water solution as a solvent, and then, preparing regenerated cellulose by using water as a coagulating bath; blending the regenerated cellulose and a starch solution, and coating after carrying out vacuum degassing. The elasticity modulus and elongation at break of the composite film are remarkably increased as comparison with those of a starch matrix. The cellulose and starch are wide in source and low in price and can be completely dissolved, so that the starch film is expected to be applied to the food packaging field.

The invention discloses a method for preparing super absorbent resin by using carboxymethyl potato starch as the raw material, which comprises the following main processes: carrying out neutralizationreaction between a sodium hydroxide solution and acrylic acid from which polymerization inhibitor is removed under the cooling of ice-water bath; mixing carboxymethyl potato starch with de-ionized water; mixing the prepared acrylic acid and the sodium salt solution thereof with the carboxymethyl potato starch solution; adding an evocating agent persulfate and a cross-linking agent N,N'- methylene-bisacrylamide; stirring the mixture under room temperature; heating the mixture by water bath to rise the temperature gradually so as to ensure that the carboxymethyl potato starch and the acrylic acid and the sodium salt thereof generate graft copolymerization reaction under the protection of nitrogen; keeping the temperature of the reaction; drying and crashing to obtain the super absorbent resin by using carboxymethyl potato starch as the raw material. Compared with similar products, the water absorption of the super absorbent resin is greatly enhanced, the process of pasting is omitted incomparison with the process of using starch as the raw material and the preparation process is greatly improved. The super absorbent resin has great effect on the water conservation, the production of the physical hygiene sundries, the environmental improvement, the desert control, the plant growth promotion and the like of soil in dry regions.

The invention discloses a preparation method of a dendrobium officinale extract. The method comprises the following steps: by taking fresh dendrobium officinale strips as a raw material, performing fermentation with neutral protease after juice squeezing; quickly freezing fermentation liquor, naturally unfreezing the fermentation liquor, and removing starch and other impurities from the fermentation liquor; removing a starch solution through treatment with strongly acidic cation exchange resin and weakly basic anion exchange resin; and finally performing concentration with a titanium stick filter, performing alcohol precipitation and centrifugation, collecting supernatant, and freeze-drying the supernatant to prepare the dendrobium officinale extract. The preparation method is simple to operate, low in cost and high in industrialization degree. The dendrobium officinale extract provided by the invention is used for preparing medicines for treating wounds. Compared with a control group, the dendrobium officinale extract is remarkably different in wound size, healing speed and mean healing time within 10 days after operation of rabbits; and the dendrobium officinale extract can speed up the healing of a wound of a wound model rabbit.

The invention provides a method for preparing amphiprotic starch solution for papermaking, which belongs to the field of fine chemicals for papermaking. The amphiprotic starch solution is added at a papermaking wet end, and has a dry strengthening effect on paper. Starch is used as the basic material, water, sodium hydroxide, sodium hypochlorite or potassium persulfate and cationic etherifying agent are added. The amphiprotic starch solution is obtained after the aqueous solution is heated. The preparation method is fulfilled by the heating reaction of aqueous solution. The amphiprotic starchsolution has high concentration, can be diluted by cold water to any concentration and cannot be aged, so the technical problem of starch aging is solved. When in use, the amphiprotic starch solutioncan be added at the wet end without being heated to gelatinize, the amphiprotic starch solution as dry-strengthening agent for papermaking can notably increase the dry strength indexes of paper, suchas burst index and ring crush index, and under the circumstance of the same added amount, the amphiprotic starch solution has a better effect than the like product. The innovation of the invention isthat a simple technique for producing the amphiprotic starch solution is provided, the production time is not longer than 2 hours, the aging and retrograding problems of the amphiprotic starch are solved, and the invented amphiprotic starch solution can be directly added at the papermaking wet end without going through the step of gelatinization by heating.

The invention discloses a process for moderate-temperature self-assembly preparation of nano starch from enzymolysis short amylose. The process particularly comprises the following steps: (1) preparing a buffer solution; (2) preparing a starch water solution; (3) past-forming; (4) enzymolyzing, and then using anhydrous ethanol to precipitate the degreased starch solution; (5) preparing short amylose; (6) preparing nano starch. According to the process, enzyme hydrolysis starch is adopted to prepare nano starch at 30-70 DEG C in an anabiosis manner, the nano starch prepared by the method is high in productivity, low in cost, safer and more environment-friendly, and can serve as embedding materials of medicines, active ingredients and the like, and the application field of the process in the food industry is widened.

The invention discloses a method for preparing fibroin nano-silver hydrosol. The method comprises the following steps of: dissolving or dispersing soluble amylose in deionized water, stirring the mixture until the amylose is completely gelatinized to obtain a starch solution, adding a silver nitrate solution, and then mixing the mixture with a fibroin solution to obtain a fibroin-starch-silver nitrate ternary complex solution; adjusting the pH value of the ternary complex solution to be at 8-10 by ammonia water, and fully mixing at the temperature condition of 20-80 DEG C to obtain the fibroin nano-silver hydrosol with the silver particle size being 1-100nm. According to the method, micromolecule fibroin peptide is used as a capturing agent and a reducing agent, the soluble starch is used as a dispersing agent and a protective agent, and the micromolecule fibroin peptide and the soluble starch are used for reducing and preparing nano-silver. The prepared nano-silver hydrosol is small in silver particle size, uniform in distribution and good in stability, in the prepared process, the reaction is mild, the operation is convenient, the green and environment-friendly aim is realized, and the fibroin nano-silver hydrosol can be widely used as a functional nano-material.

The present invention relates to a bound metal oxide particle comprised of metal oxide and a binder, with the binder preferably being a starch solution. The present invention also relates to a method for forming a bound metal oxide particle, with the preferred method including extruding and pelletizing a metal oxide and binder composition to form pelletized metal oxide particles.

The invention discloses multifunctional microporous styptic powder and a preparation method and application thereof. The preparation method comprises the following steps: 1) mixing starch with water to obtain a starch solution or starch pasty liquid; 2) mixing carboxymethyl chitosan with water to obtain a carboxymethyl chitosan solution; 3) mixing the starch solution or the starch pasty liquid with the carboxymethyl chitosan solution to obtain a blended solution; 4) dispersing a pore-forming agent into the blended solution to obtain blended dispersion liquid; 5) dropwise adding an ionic crosslinker into the blended dispersion liquid under a stirring condition, mixing the obtained mixed system with a dispersing agent and an emulsifying agent, and performing crosslinking reaction and suction filtration; 6) removing the pore-forming agent from a product obtained in the step 5), and drying; 7) performing microwave treatment on a product obtained in the step 6) to obtain the styptic powder. The preparation method adopts a dual crosslinking method of ionic crosslinking and microwave treatment; used reagents are environmentally friendly, and free of residues; the biological activity of an amino group in the carboxymethyl chitosan can be retained easily.

The invention relates to a host cell and a method for the host cell applied in efficient secretion expression of a recombinant protein, which belongs to the filed of microbiological engineering and fermentation engineering. The invention provides a bacillus licheniformis host cell CBB3008 which is preserved in the China Center for Type Culture Collection with the preserving number of CCTCC NO: M 208236. The invention transforms an expression plasmid of an industrial enzyme which is obtained by a gene cloning technology into the host cell to synthesize an industrial enzyme preparation in the host cell efficiently, and then secretes the synthesized enzyme protein into a culture medium efficiently through a protein secretion system of the host cell, thus the invention can guide efficient secretion production of the industrial enzyme preparation. Therefore, the invention is helpful to reduce the fermentative production cost of the industrial enzyme preparation, simplify the fermentative production process and reduce the environmental pressure of the fermentation industry. A method for host cell screening and genetic improvement of the invention can also be used for other types of host cells, in particular for the breeding of the host cells of bacillus subtilis, bacillus megaterium, bacillus pumilus, bacillus starch solution and the like.

The invention relates to a multiphase Fenton catalyst as well as a preparation method and application thereof and mainly solves the technical problems of poor mechanical strength and high ion solubility of an existing multiphase Fenton catalyst. The multiphase Fenton catalyst is prepared from reduced iron powder, active carbon powder, electrolytic copper powder and silicate. The preparation method comprises the following steps: (1) weighing the reduced iron powder, the active carbon powder, the electrolytic copper powder and the silicate; (2) firstly mixing the active carbon powder and the electrolytic copper powder to be uniform, then adding a silicate solution, mixing to be uniform, adding the active carbon powder, and mixing to be uniform so as to obtain mixed powder; (3) adding a starch solution serving as a binding agent into the mixed powder to prepare granules and drying; (4) sintering in nitrogen atmosphere, so as to obtain the multiphase Fenton catalyst. The multiphase Fenton catalyst prepared by utilizing the preparation method can be used as a sewage treatment catalyst.

Systems and methods are provided for separating high value by-products, such as oil and/or germ, from grains used for alcohol production. In one embodiment, a method for separating by-products from grains used for alcohol production includes, subjecting milled grains to liquefaction to provide a liquefied starch solution including fiber, protein, and germ. The germ is separated from the liquefied starch solution. The separated germ is ground, e.g., to a particle size less than 50 microns, to release oil to provide a germ/oil mixture. Then, prior to fermentation, the oil is separated from the germ/oil mixture to yield an oil by-product. The pH of the germ/oil mixture can be adjusted to about 8 to about 10.5 and/or cell wall breaking enzymes or chemicals may be added to help release oil from the germ. In one example, the oil yield is greater than 1.0 lb/Bu.

The invention discloses a preparation method of a starch-based composite flocculant and application thereof. The method is characterized by taking sodium silicate, aluminium salt and iron salt as main raw materials and water as a reaction solvent to prepare ferro-silico aluminium and compounding an alkaline modified starch solution with the ferro-silico aluminium to prepare the starch-based composite flocculant. The starch-based composite flocculant is mainly applied to printing and dyeing wastewater treatment. The starch-based composite flocculant has the advantages of high decolorization rate and CODCr removal rate, high sedimentation velocity, less sludge quantity and no secondary pollution.

The invention relates to a preparation method of a p-aramid fiber-mica paper. The preparation method comprises defibering and dispersing silane coupling agent-modified p-aramid chopped fibers to obtain slurry A, carrying out screening on the p-aramid fibrids with a beating degree of 40-65 degrees SR to obtain slurry B, modifying mica plates through an ionic starch solution to obtain modified mica plates, mixing the slurry A, the slurry B and the modified mica plates to obtain uniform mixed slurry, wherein the uniform mixed slurry comprises, by mass, 10-20% of p-aramid chopped fibers, 20-40% of the p-aramid fibrids and 40-70% of the mica plates, carrying out sizing, dehydration and formation on the mixed slurry, carrying out squeezing and drying and carrying out hot press molding to obtain the p-aramid fiber-mica paper. The p-aramid fiber-mica paper obtained through fiber screening and modification, wet method paper making and hot pressing molding has good evenness, excellent mechanical strength, excellent dielectric breakdown strength and high temperature resistance stability.

The invention relates to an edible package film based on chitosan and a preparation method thereof. At present, industrial production and actual commercial application of the edible package film are not promoted due to the most important reasons that the edible package film is poor in mechanical strength and has no hot-sealing property. In the invention, a calendering method is employed, wherein the preparation method includes the steps of: mixing a chitosan solution with a gelatin solution or a starch solution, adding glycerol, propolis and lysozyme, performing temperature-constant blend cooling and then ultrasonic degassing, and allowing the mixture to stand to prepare a composite film liquid; and spreading the composite film liquid in a flat dish, and vacuum-drying the film liquid to prepare the edible package film. Through addition of the gelatin, the starch and the like bio-macro-molecular components, the film-forming performance of the chitosan is improved. The chitosan composite film is improved in mechanical performance, and meanwhile, with addition of the natural anti-bacterial components, propolis and lysozyme, which have synergistic effects, the chitosan composite film, as food packages, can inhibit reproduction of microorganisms and prolong the shelf life of the foods largely, so that the edible package film can be used in industrial production and has a wide application prospect.

The invention relates to a method for preparing a Lactobacillus casei microcapsule. 2-6 percent of microporous starch solution and 2-6 percent of sodium alginate solution are respectively taken as inner and outer wall materials of the microcapsule; the characteristic that small holes overspread on the surface of the microporous is utilized to absorb a bacteria solution; then sodium alginate and calcium chloride are utilized to generate ion exchange to form a sodium alginate coating; and double layer embedment is carried out on Lactobacillus casei. After the Lactobacillus casei microcapsule is dried at the temperature of 2-6 DEG C for 36-72h, the obtained microcapsule has stronger acid resistance and cholate resistance and high storage stability, i.e. the microcapsule is not dissolved in simulated gastric fluid basically and does not leak but is immediately disintegrated in simulated intestinal fluid; after the Lactobacillus casei microcapsule is treated in 0.3 percent of cholate solution for 1h, the thalli survival rate is 88 percent, and the number of viable bacteria is increased to 1.24*109cfu/g from 5.80*109cfu/g after the Lactobacillus casei microcapsule is stored at the temperature of 4 DEG C for 1 month. The invention greatly increases the survival rate of Lactobacillus casei in products and the use ratio of Probiotics and also enriches the variety of the Probiotics microcapsule.

The invention discloses a preparation method of a hydrophilic polymer-modified polyurethane foaming plastic carrier. The preparation method comprises steps of: 1) cutting polyurethane flexible foam into pieces; 2) preparing an aqueous starch solution having a proper concentration, an aqueous sodium carboxymethylcellulose solution having a proper concentration, a N,N-dimethyl formamide solution of polybutanimide having a proper concentration; 3) dipping polyurethane foaming plastic into the aqueous starch solution, the aqueous sodium carboxymethylcellulose solution and the N,N-dimethyl formamide solution of the polybutanimide; and then transferring the polyurethane foaming plastic into an aqueous cross-linking agent solution and heating; and 4) taking the foaming plastic out, washing and drying. The preparation method is simple in technology and convenient in operation. A microbial carrier which has an advantage of cost performance and is used for sewage treatment can be obtained after modification.

The invention discloses a disinfectant health-care aromatic hand paper towel and a preparation method thereof. The hand paper towel comprises the following components: softwood sulfite pulp, bamboo-pulp paper fiber, straw pulp, a cationic starch solution, a wet strength agent, a powerful antibacterial agent, an aromatic agent and titanium dioxide, wherein the wet strength agent is polyethylene ethylamine resin, the powerful antibacterial agent is composed of pure-oxygen-based quaternary ammonium salt, Sophora flavescens, common cnidium fruit, honeysuckle, borneol, isatis root, ethanol and distilled water, and the aromatic agent is composed of chitosan, ethanol, essence extract, deionized water, glycerin and triphosphoric acid. The prepared disinfectant health-care aromatic hand paper towel in the invention has the characteristics of no toxicity, harmlessness, environmental protection, highly-efficient antibacterial property and emission of aroma, can efficiently avoid contact-type cross infection with bacteria in public places and is safer and more secure to use.

The invention discloses a method for preparing a novel solid acid catalyst. The method adopts porous high temperature-resistance media as carriers and includes adding soluble sugar or starch solution; evaporating to dryness for a plurality of times; igniting; washing in water; drying; reacting with concentrated sulfuric acid; washing until a neutral condition with hot water; filtering; and drying to obtain the novel solid acid catalyst. The obtained solid acid catalyst is linked with sulfonic groups and loaded on the porous high temperature-resistance medium based on hydrophobic amorphous carbon structure prepared by calcining different glycosyl groups, and has the advantages of porosity, large specific surface area, even particle size and easy separation and filling into a tubular reactor. The catalyst has an activity higher than the conventional solid acid catalyst which can be reutilized and easily recovered and is an excellent catalyst for preparing biodiesel oil from waste edible oil such as trench oil and acidification oil.

The invention discloses a starch-based porous hydrogel prepared from a starch liquid, an initiating agent, a monomer and a cross-linking agent. The preparation method comprises the following steps: adding the initiating agent, the monomer and cross-linking agent into the starch liquid; after each component is added, mixing uniformly, and heating for full reaction, thereby obtaining a starch-based hydrogel; and washing and swelling the obtained starch-based hydrogel, immerging the washed and swelled starch-based hydrogel into an organic solvent-water mixed solution with specific components so as to perform gradient solvent exchange, and drying, thereby obtaining the starch-based porous hydrogel. The starch-based porous hydrogel has the characteristics of simple and convenient preparation method, good open pore property, controllable porous structure and stable three-dimensional structure.