Preparation method for activated alumina with large pore volume and high specific surface area
A high specific surface area, activated alumina technology, applied in the direction of alumina/hydroxide preparation, chemical instruments and methods, catalyst supports, etc., can solve the complex process and the difficulty of activated alumina to simultaneously exert large pore volume and high specific surface area , high production costs, etc., to achieve the effect of simple process, large pore size and low cost of raw materials
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[0014] Example 1: Take 100ml of 1mol / L nitric acid solution and place it in a beaker, set the water bath reaction temperature to 30°C and perform magnetic stirring, slowly drip the sodium aluminate solution (αk=1.45) into the above solution until The pH of the solution reaches 10. Set the aging temperature to 60°C and perform vigorous stirring for aging, and the aging time is 2h. After aging, vacuum filtration was used to separate solid-liquid and ultrasonically washed several times. The obtained filter cake was transferred to a distillation flask, and n-butanol was added in a ratio of solid-liquid volume ratio = 1:5 for co-distillation. The obtained activated alumina precursor was put into a muffle furnace and calcined at 500°C for 4 hours to obtain activated alumina with large pore volume and high specific surface area.
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[0015] Example 2: Take 100ml, 1mol / L nitric acid solution and place it in a beaker, set the water bath reaction temperature to 30°C and perform magnetic stirring, slowly drip the sodium aluminate solution (αk=1.40) into the above solution until The pH of the solution reaches 9. Set the aging temperature to 70°C and perform vigorous agitation for aging. The aging time is 4h. After aging, vacuum filtration was used to separate solid-liquid and ultrasonically washed several times. The obtained filter cake was transferred to a distillation flask, and n-butanol was added in a ratio of solid-liquid volume ratio=1:4 for co-distillation. The obtained activated alumina precursor was put into a muffle furnace and calcined at 500°C for 4 hours to obtain activated alumina with large pore volume and high specific surface area.
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[0016] Example 3; Take 100ml of 2mol / L nitric acid solution and place it in a beaker, set the water bath reaction temperature to 20°C and perform magnetic stirring, slowly drip the sodium aluminate solution (αk=1.35) into the above solution until The pH of the solution reached 9. Set the aging temperature to 80°C and perform vigorous agitation for aging. The aging time is 5h. After aging, vacuum filtration was used for solid-liquid separation and ultrasonic washing several times, the obtained filter cake was transferred to a distillation flask, and n-butanol was added in a ratio of solid-liquid volume ratio = 1:5 for co-distillation. The obtained activated alumina precursor was put into a muffle furnace and calcined at 500°C for 4 hours to obtain activated alumina with large pore volume and high specific surface area.
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