Method for preparing high-specific-surface-area activated carbon from tobacco stalks
A high specific surface area, activated carbon technology, used in chemical instruments and methods, solid waste removal, inorganic chemistry, etc. problems, to achieve the effect of saving process time and energy, easy control, and fast carbonization reaction
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Embodiment 1
[0026] After crushing the tobacco stem waste, take 150-mesh particles, mix the particles and KOH at a weight ratio of 2:1, add water and soak for 14 hours, stir thoroughly, filter, and vacuum-dry at 100°C for 3 hours, then put the dried mixture in Under the protection of nitrogen, use a tubular electric furnace to heat up to 600°C at a heating rate of 12°C / min, keep it for 1.5h, then cool and wash to pH=7, then vacuum dry at 100°C for 3h, and grind to obtain activated carbon products.
[0027] The main index of the tested product activated carbon is the specific surface area of 852sq m / g, and the micropores and mesopores account for 76% of the total pore volume.
Embodiment 2
[0029] After the tobacco stem waste is crushed, take particles of about 150 meshes, mix the particles and KOH at a mass ratio of 1:4, add water and stir thoroughly, filter after soaking for 12 hours, and vacuum-dry at 105°C, and then dry the dried mixture Under the protection of nitrogen, use a tubular electric furnace to heat up to 480°C at a heating rate of 15°C / min, keep it for 1.5h, then cool and wash to pH=7, then vacuum dry at 100°C for 3h, and grind to obtain activated carbon products . The main index of the tested product activated carbon is the specific surface area of 1208sq m / g, and the micropores and mesopores account for 82% of the total pore volume.
Embodiment 3
[0031] Take about 150 mesh particles and K 2 CO 3 Mix according to the mass ratio of 1:1, add water and stir thoroughly, impregnate for 12 hours, filter, vacuum dry at 105°C, and then heat the dried mixture with a tubular electric furnace at a rate of 10°C / min under nitrogen protection Heating to 500°C, keeping it for 1.5h, then cooling, washing to pH=7, vacuum drying at 105°C for 3h, and grinding to obtain the activated carbon product. The main index of the tested product activated carbon is the specific surface area of 1150sq m / g, and the micropores and mesopores account for 88% of the total pore volume.
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