Pharmaceutical composition of lappaconitine hydrobromide
A technology of homogenin hydrobromide and composition, which is applied in the direction of drug combination, drug delivery, antipyretic, etc., which can solve the problems of poor taste, high incidence, inconvenient use, etc., and achieve good stability
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Embodiment 1
[0031] The preparation of embodiment 1, homogenine hydrobromide spray
[0032] Weigh 0.03g of methyl p-hydroxybenzoate, put it in a 100mL volumetric flask, add an appropriate amount of water for injection, heat it in a warm water bath to dissolve, cool to room temperature, then add 1.0g of uricine hydrobromide, 2g of citric acid, stevia Glycoside 0.5mg, sidimenthol 2.0g, shake to dissolve, add water for injection near the mark, shake well, adjust to pH 4.0 with 0.1M sodium hydroxide (or 0.1M hydrochloric acid if necessary), and then inject Water to the mark, shake well, and filter with 0.45 μm microporous membrane to obtain homogenate hydrobromide spray solution, which is then filled in a single-dose or multi-dose spray device, and packed for later use.
[0033] Described sidimenthol is prepared by the ratio of HP-β-cyclodextrin (referred to as β-CD in the following steps) and Menthol with a weight ratio of 125:20, and its detailed preparation steps are as follows:
[0034]...
Embodiment 2
[0037] The preparation of embodiment 2, homogenine hydrobromide spray
[0038] Weigh 0.05g of propyl p-hydroxybenzoate, put it in a 100mL volumetric flask, add 20g of propylene glycol, add an appropriate amount of water for injection, heat in a warm water bath to dissolve, cool to room temperature, and then add 1.0g of homogenin hydrobromide, citrate Citric acid 1g, stevioside 0.5mg, menthol (see Example 1 for preparation) 2.0g, shake to dissolve, add water for injection near the mark, shake well, and use 0.1M sodium hydroxide (or if necessary, use 0.1 M hydrochloric acid) to adjust to pH 4.5, add water for injection to the scale, shake well, and filter with 0.45 μm microporous membrane to obtain homogenin hydrobromide spray liquid, which can then be filled in single dose or multi-dose Dosage spray device, packed ready for use.
Embodiment 3
[0039] Embodiment 3, the preparation of homogenin hydrobromide aqueous solution
[0040]Take 0.2 g of uricine hydrobromide, 4 g of sodium citrate, and 1 g of tartaric acid, add water to about 90 ml, dissolve, and adjust the pH value to 3.5 with 0.1 M hydrochloric acid (or 0.1 M sodium hydroxide if necessary), Add water for injection to 100ml, shake well, and get ready.
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