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Method for preparing biological aviation fuel by using litsea cubeba kernel oil

A technology of aviation fuel and litsea cubeba oil, applied in the field of preparing bio-aviation fuel from litsea cubeba fruit seed oil, achieving good economic and social benefits and improving quality

Inactive Publication Date: 2012-10-10
WEIMING BIO ENERGY CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, there is currently no method for preparing bio-aviation fuel from litsea cubeba seed oil

Method used

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  • Method for preparing biological aviation fuel by using litsea cubeba kernel oil

Examples

Experimental program
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Effect test

Embodiment 1

[0029] This embodiment includes the following steps:

[0030] (1) Filter the litsea cubeba fruit pit oil to remove particulate impurities, add softened water at the same temperature at 70°C, the weight of the added softened water is equivalent to 5% of the weight of litsea cubeba oil, stir for 30 minutes, and then Centrifuge at a speed of 3000r / min for 30 minutes, take the supernatant, and dry it in a vacuum oven at 103°C for 3 hours to obtain refined litsea cubeba oil;

[0031] (2) After cooling the refined litsea cubeba fruit stone oil obtained in step (1), it is introduced into a fixed-bed hydrogenation reaction device filled with a hydrodeoxygenation catalyst to carry out a hydrodeoxygenation reaction; the hydrodeoxygenation catalyst is NiO- WO 3 / Aluminosilicate molecular sieve supported catalyst, the dosage is equivalent to 3% of the weight of the obtained refined Litsea cubeba oil, the temperature is raised to 350°C, the absolute pressure is 4MPa, and hydrogen is introd...

Embodiment 2

[0037] This embodiment includes the following steps:

[0038] (1) Filter the Litsea cubeba fruit kernel oil to remove particulate impurities, add softened water at the same temperature at 70°C, the weight of the added softened water is equivalent to 5% of the weight of Litsea cubeba oil, stir for 30 minutes, and then Centrifuge at a speed of 3000r / min for 30 minutes, take the supernatant, and dry it in a vacuum oven at 103°C for 3 hours to obtain refined litsea cubeba oil;

[0039] (2) After cooling the refined litsea cubeba fruit stone oil obtained in step (1), it is introduced into a fixed-bed hydrogenation reaction device filled with a hydrodeoxygenation catalyst to carry out a hydrodeoxygenation reaction; the hydrodeoxygenation catalyst is equivalent to the obtained Refined litsea cubeba oil weight 2% CoO-MoO 3 / γ-Al 2 o 3 Supported catalyst, the temperature is raised to 320°C, the absolute pressure is 3MPa, and hydrogen is introduced at the same time, the hydrogen-oil ...

Embodiment 3

[0043] This embodiment includes the following steps:

[0044] (1) Filter the Litsea cubeba fruit kernel oil to remove particulate impurities, add softened water at the same temperature at 70°C, the weight of the added softened water is equivalent to 5% of the weight of Litsea cubeba oil, stir for 30 minutes, and then Centrifuge at a speed of 3000r / min for 30 minutes, take the supernatant, and dry it in a vacuum oven at 103°C for 4 hours to obtain refined litsea cubeba oil;

[0045] (2) After cooling the refined litsea cubeba fruit stone oil obtained in step (1), it is introduced into a fixed-bed hydrogenation reaction device filled with a hydrodeoxygenation catalyst to carry out a hydrodeoxygenation reaction; the hydrodeoxygenation catalyst is equivalent to the obtained Refined litsea cubeba oil weight 5% NiO-MoO 3 / γ-Al 2 o 3 Supported catalyst, the temperature is raised to 350°C, the absolute pressure is 3.5MPa, and hydrogen is introduced at the same time, the volume rati...

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Abstract

The invention discloses a method for preparing biological aviation fuel by using litsea cubeba kernel oil, comprising the following steps of: (1) refining the litsea cubeba kernel oil; (2) introducing the refined litsea cubeba kernel oil into a fixed-bed hydrogenation reaction device and sequentially carrying out hydrogenation and deoxygenation reaction and isomerization reaction; (3) collecting liquid-phase components through a condenser; (4) distilling and collecting distillate with the temperature of 150-280 DEG C; and (5) refining the collected distillate through a fiber liquid membrane-composite adsorption unifying device and a dielectric field refining device to obtain the biological aviation fuel meeting the aviation fuel specification. By using the method, the obtained biological aviation fuel contains no sulfur and arene and is good in quality, high in cleanliness and environment-friendly.

Description

technical field [0001] The invention relates to a method for preparing bio-aviation fuel, in particular to a method for preparing bio-aviation fuel by utilizing litsea cubeba fruit stone oil. Background technique [0002] At present, all countries in the world are facing the dual challenges of energy crisis and climate change. With the depletion of fossil energy, biofuels have gradually entered the field of vision of mankind. Because traditional resources such as coal, oil, and natural gas burn the carbon fixed in the interior of the earth and emit it into the atmosphere, their utilization will inevitably increase the content of carbon dioxide in the atmosphere, thereby intensifying the greenhouse effect of the earth. The formation of biomass is the process by which plants convert carbon dioxide already present in the atmosphere into glucose and then into plants through the photosynthesis of chlorophyll. This process can effectively reduce the carbon dioxide content in the a...

Claims

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Application Information

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IPC IPC(8): C11C1/02C11C1/08C10L1/02
Inventor 朱岳麟袁遥尹雨晨廖斌
Owner WEIMING BIO ENERGY CO LTD
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