Acidification preflushing fluid with seepage regulatory function

A technology of seepage and regulator, applied in the direction of drilling composition, chemical instruments and methods, etc., can solve problems such as insufficient acidification of production layers, impact on oil well productivity, and ineffective acid fluid, so as to improve development efficiency or economic benefits, The effect of prolonging the stable production period and reducing production costs

Inactive Publication Date: 2012-10-17
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] During the implementation of conventional acidizing process in oil field development, the traditional pre-fluid is generally deionized water or deionized water with active agent added. This pre-fluid plays a role in the acidizing treatment of production wells, but at the same time there are the following problems Disadvantages or deficiencies: ① When acidizing oil wells with heterogeneity and large interlayer permeability differences, the acid liquid first enters the high permeability layer, and often the subsequent acid liquid is ineffective or ineffi

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] Phase permeability modifier: a. Add 5 parts of acrylic acid monomer, 2 parts of acrylate monomer, 1 part of acrylamide monomer, 2 parts of coupling agent KH570 monomer, and 90 parts of deionized water into the reactor in sequence, and stir evenly ; b, heated to 90 ° C constant temperature; c, nitrogen gas and stirred for 30 minutes to remove the oxygen in the solution; d, adding a solid initiator with a mass percentage content of 0.2%, the solid initiator is sodium bisulfite and sodium bisulfite with a mass ratio of 1:1 Ammonium persulfate was initiated under normal pressure to carry out polymerization reaction, and the reaction was carried out for 7 hours to obtain the target product with a molecular weight of 7 million. The solid initiator is sodium bisulfite and ammonium persulfate with a mass ratio of 1:1.

[0022] The acidified preflush with the function of seepage adjustment is prepared by adding 20Kg of a phase permeability regulator with a mass percentage of 0.2...

Embodiment 2

[0024] Phase permeability modifier: a. Add 10 parts of acrylic acid monomer, 6 parts of acrylate monomer, 4 parts of acrylamide monomer, 4 parts of KH570 monomer, and 76 parts of deionized water into the reactor in sequence, and stir evenly; b. Heating to a constant temperature of 90°C; c, stirring with nitrogen for 30 minutes to remove oxygen in the solution; d, adding a solid initiator with a mass percentage content of 0.4%, and the solid initiator is sodium bisulfite and ammonium persulfate with a mass ratio of 1:2 , Initiate it to carry out polymerization reaction under normal pressure, react for 8 hours, obtain the target product, its molecular weight is 7 million.

[0025] The acidification preflux with the function of seepage adjustment is prepared by adding 300Kg of a phase permeability regulator with a mass percentage of 2% per 10,000 kg of clear water, and stirring evenly under normal temperature and pressure; or adding mass percent per 10,000 kg of clear water 300Kg...

Embodiment 3

[0027] Phase permeability modifier: a. Add 15 parts of acrylic acid monomer, 8 parts of acrylate monomer, 8 parts of acrylamide monomer, 5 parts of KH570 monomer, and 64 parts of deionized water into the reactor in sequence, and stir evenly; b. Heat to a constant temperature of 90°C; c. Stir with nitrogen gas for 30 minutes to remove oxygen in the solution; d. Add mass 100

[0028] A solid initiator with a proportion content of 0.8%, the solid initiator is sodium bisulfite and ammonium persulfate with a mass ratio of 1:3, triggers it to carry out polymerization reaction under normal pressure, reacts for 9 hours, obtains the target product, and its molecular weight is seven million.

[0029] The preparation method of acidified prefluid with seepage regulation function is as follows: add 500Kg of phase permeability regulator with a mass percentage of 5% per 10,000 kg of clear water, and stir evenly under normal temperature and pressure; 500Kg of phase permeability regulator wit...

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PUM

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Abstract

An acidification preflushing fluid with a seepage regulatory function comprises a seepage regulatory agent and an acidification preflushing fluid. The preparation technology for the seepage regulatory agent comprises: adding 5-15 parts by weight of acrylic acid monomer, 2-8 parts by weight of acrylic acid ester, 1-8 parts by weight of acrylamide and 2-5 parts by weight of coupling agent KH570, and the balance deionized water successively to a reaction vessel, stirring to uniform, heating to 90 DEG C and keeping constant temperature, stirring as feeding nitrogen for 30min to remove oxygen in the solution, and adding a solid initiator with a mass percentage content of 0.2%-0.8% to initiate the solution to carry out a polymerization reaction at normal pressure for 7-9 h. A preparation method for the acidification preflushing fluid is that: the preflushing fluid is formed by adding a phase permeability modifier with a mass percent of 0.2%-5% to deionized water or clear water and stirring to uniform at normal temperature and pressure, or adding the phase permeability modifier with a mass percentage of 0.2%-5%, a corrosion inhibitor with a mass percentage of 0.5%-2% and hydrochloric acid or mud acid with a mass percentage of 5%-20% to deionized water or clear water and stirring to uniform at normal temperature and pressure.

Description

technical field [0001] The invention relates to a method for water-controlled acidification of water-bearing oil wells in oilfield development, in particular to an acidification pre-fluid with seepage regulation function. Background technique [0002] During the implementation of conventional acidizing process in oil field development, the traditional pre-fluid is generally deionized water or deionized water with active agent added. This pre-fluid plays a role in the acidizing treatment of production wells, but at the same time there are the following problems Disadvantages or deficiencies: ① When acidizing oil wells with heterogeneity and interlayer permeability differences, the acid liquid first enters the high permeability layer, and often the subsequent acid liquid is ineffective or inefficient, resulting in insufficient acidification of the production layer and affecting Acidizing effect; ②Acidizing often has the phenomenon that the water content rises rapidly after con...

Claims

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Application Information

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IPC IPC(8): C09K8/588
Inventor 王登庆宋金波梅明霞孙秀钊郑铎许霞姜静武明鸣杨军
Owner CHINA PETROLEUM & CHEM CORP
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