Refining method of starch sugar liquor
A refining method, starch sugar technology, applied in separation methods, chemical instruments and methods, solid adsorbent liquid separation, etc., can solve problems such as difficult to effectively remove silicon compounds, and achieve effective anion exchange, selectivity enhancement, extreme sex-enhancing effect
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Embodiment 1
[0092] 1) Take two plexiglass chromatography columns (volume 400ml, diameter 20mm), fill them with 280ml cation resin A and anion resin A respectively, and connect the two chromatography columns filled with resin in series. The column with cation resin A is on top.
[0093] 2) At a temperature of 40°C, 100L starch sugar solution (the content of starch sugar (based on the total amount of glucose, fructose and maltose) is 40% by weight, the content of silicon compound (calculated as silicon dioxide) 40ppm, metal cation content (as Mg 2+ , Ca 2+ and Fe 3+ total content) is 50ppm, the chromaticity of starch sugar solution is 50 degrees) at a speed of 3.6 times the volume of cation resin per hour through the series of chromatographic columns, and the solution that has just passed through the separation column equipped with cations is analyzed every 1 hour Take a sample once and determine the content of metal cations (as Mg 2+ , Ca 2+ and Fe 3+ total content), the maximum cont...
Embodiment 2
[0095] 1) Take two plexiglass chromatography columns (volume 600ml, diameter 50mm), fill them with 450ml cation resin B and anion resin B respectively, and connect the two chromatography columns filled with resin in series, among them, The column with cation resin B is on top.
[0096] 2) At a temperature of 50°C, 100L starch sugar solution (the content of starch sugar (based on the total amount of glucose, fructose and maltose) is 30% by weight, the content of silicon compound (calculated as silicon dioxide) 110ppm, metal cation content (as Mg 2+ , Ca 2+ and Fe 3+ total content) is 200ppm, and the chromaticity of starch sugar solution is 20 degrees) at a speed of 2.5 times the volume of cation resin per hour through the series of chromatographic columns, and every 1 hour the solution that has just passed through the separation column equipped with cations Take a sample once and determine the content of metal cations (as Mg 2+ , Ca 2+ and Fe 3+ total content), the maximu...
Embodiment 3
[0098] 1) Take two plexiglass chromatography columns (volume 500ml, diameter 30mm), fill them with 350ml cation resin C and anion resin C respectively, and connect the two chromatography columns filled with resin in series, among them, The column with cation resin C is on top.
[0099] 2) At a temperature of 60°C, 100L of starch sugar solution (the content of starch sugar (based on the total amount of glucose, fructose and maltose) is 35% by weight and the content of silicon compounds (calculated as silicon dioxide) 70ppm, metal cation content (as Mg 2+ , Ca 2+ and Fe 3+ total content) is 100ppm, and the color of starch sugar solution is 35 degrees) at a rate of 2.85 times the volume of cation resin per hour through the series of chromatographic columns, and the solution that has just passed through the separation column equipped with cations is analyzed every 1 hour Take a sample once and determine the content of metal cations (as Mg 2+ , Ca 2+ and Fe 3+ total content),...
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