Low-temperature sintered zirconium silicate grinding ball and preparation method thereof
A technology of low-temperature sintering and zirconium silicate, which is applied in chemical instruments and methods, and other chemical processes, and can solve problems such as small size, poor particle size uniformity, and fragile grinding balls
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Embodiment 1
[0016] The mass percentage of zirconium silicate is 60%, the mass percentage of alumina is 30%, the mass percentage of silicon oxide is 2%, the mass percentage of yttrium oxide is 0.5%, the mass percentage of calcium carbonate is 2%, the potassium carbonate mass percentage is 5%, the carbonic acid Sodium mass percentage is 0.5%. After mixing the above raw material powders in proportion, add water and grinding medium, the mass ratio of raw material powder: water: grinding medium is 1:1.5:3. After ball milling, a uniformly mixed slurry is obtained, then ground for a period of time by a vertical sand mill to obtain a slurry that meets the requirements, and then dried to obtain raw material powder. The raw material powder and binder are sprayed into the ball rolling machine, and the green green ball with the required diameter is formed by the rolling ball machine. The green body ball is sintered to obtain a zirconium silicate ball with a diameter of about 2 mm. The sintering pro...
Embodiment 2
[0018] The mass percentage of zirconium silicate is 65%, the mass percentage of alumina is 2%, the mass percentage of silicon oxide is 2%, the mass percentage of yttrium oxide is 3%, the mass percentage of calcium carbonate is 5%, the mass percentage of zirconia is 20%, the carbonic acid The mass percentage of magnesium is 1%, the mass percentage of potassium carbonate is 0.5%, and the mass percentage of sodium carbonate is 1.5%. After mixing the above raw material powders in proportion, add water and grinding medium, the mass ratio of raw material powder: water: grinding medium is 1:1.5:3. After ball milling, a uniformly mixed slurry is obtained, then ground for a period of time by a vertical sand mill to obtain a slurry that meets the requirements, and then dried to obtain raw material powder. The raw material powder and binder are sprayed into the ball rolling machine, and the green green ball with the required diameter is formed by the rolling ball machine. The green body...
Embodiment 3
[0020] The mass percentage of zirconium silicate is 60%, the mass percentage of silicon oxide is 30%, the mass percentage of yttrium oxide is 0.5%, the mass percentage of calcium carbonate is 0.5%, the mass percentage of magnesium carbonate is 5%, and the mass percentage of potassium carbonate is 2%. Sodium mass percentage is 2%. After mixing the above raw material powders in proportion, add water and grinding medium, the mass ratio of raw material powder: water: grinding medium is 1:1.5:3. After ball milling, a uniformly mixed slurry is obtained, then ground for a period of time by a vertical sand mill to obtain a slurry that meets the requirements, and then dried to obtain raw material powder. The raw material powder and binder are sprayed into the ball rolling machine, and the green green ball with the required diameter is formed by the rolling ball machine. The green body ball is sintered to obtain a zirconium silicate ball with a diameter of about 2 mm. The sintering pr...
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