Low-temperature sintered zirconium silicate grinding ball and preparation method thereof

A technology of low-temperature sintering and zirconium silicate, which is applied in chemical instruments and methods, and other chemical processes, and can solve problems such as small size, poor particle size uniformity, and fragile grinding balls

Active Publication Date: 2012-11-28
江苏金石研磨有限公司
View PDF5 Cites 20 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The Chinese patent application number 99118965.6 discloses a method for preparing zirconium silicate microspheres by zirconium quartz fusion method, but the grinding balls prepared by the fusion method are prone to internal defects and are fragile, and the size is small and the particle size uniformity is poor
[0005] Application No. 201010122895.8 discloses a method of producing zirconium silicate balls after isostatic pressing and sintering at high temperature. This method is costly (isostatic pressing, high temperature) and can only be made into large balls

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] The mass percentage of zirconium silicate is 60%, the mass percentage of alumina is 30%, the mass percentage of silicon oxide is 2%, the mass percentage of yttrium oxide is 0.5%, the mass percentage of calcium carbonate is 2%, the potassium carbonate mass percentage is 5%, the carbonic acid Sodium mass percentage is 0.5%. After mixing the above raw material powders in proportion, add water and grinding medium, the mass ratio of raw material powder: water: grinding medium is 1:1.5:3. After ball milling, a uniformly mixed slurry is obtained, then ground for a period of time by a vertical sand mill to obtain a slurry that meets the requirements, and then dried to obtain raw material powder. The raw material powder and binder are sprayed into the ball rolling machine, and the green green ball with the required diameter is formed by the rolling ball machine. The green body ball is sintered to obtain a zirconium silicate ball with a diameter of about 2 mm. The sintering pro...

Embodiment 2

[0018] The mass percentage of zirconium silicate is 65%, the mass percentage of alumina is 2%, the mass percentage of silicon oxide is 2%, the mass percentage of yttrium oxide is 3%, the mass percentage of calcium carbonate is 5%, the mass percentage of zirconia is 20%, the carbonic acid The mass percentage of magnesium is 1%, the mass percentage of potassium carbonate is 0.5%, and the mass percentage of sodium carbonate is 1.5%. After mixing the above raw material powders in proportion, add water and grinding medium, the mass ratio of raw material powder: water: grinding medium is 1:1.5:3. After ball milling, a uniformly mixed slurry is obtained, then ground for a period of time by a vertical sand mill to obtain a slurry that meets the requirements, and then dried to obtain raw material powder. The raw material powder and binder are sprayed into the ball rolling machine, and the green green ball with the required diameter is formed by the rolling ball machine. The green body...

Embodiment 3

[0020] The mass percentage of zirconium silicate is 60%, the mass percentage of silicon oxide is 30%, the mass percentage of yttrium oxide is 0.5%, the mass percentage of calcium carbonate is 0.5%, the mass percentage of magnesium carbonate is 5%, and the mass percentage of potassium carbonate is 2%. Sodium mass percentage is 2%. After mixing the above raw material powders in proportion, add water and grinding medium, the mass ratio of raw material powder: water: grinding medium is 1:1.5:3. After ball milling, a uniformly mixed slurry is obtained, then ground for a period of time by a vertical sand mill to obtain a slurry that meets the requirements, and then dried to obtain raw material powder. The raw material powder and binder are sprayed into the ball rolling machine, and the green green ball with the required diameter is formed by the rolling ball machine. The green body ball is sintered to obtain a zirconium silicate ball with a diameter of about 2 mm. The sintering pr...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
densityaaaaaaaaaa
densityaaaaaaaaaa
Vickers hardnessaaaaaaaaaa
Login to view more

Abstract

The invention relates to a low-temperature sintered zirconium silicate grinding ball and a preparation method thereof, relating to a grinding medium. The raw materials of the ball are as follows: zirconium silicate as the substrate material; and a combination of alumina, silicon oxide, zirconia, yttrium oxide, calcium carbonate, magnesium carbonate, potassium carbonate and sodium carbonate as a sintering aid. The raw materials are prepared according to an appropriate mass ratio, and go through ball milling using a ball mill, and high speed grinding by a vertical sand mill then drying to obtain raw material powder for the preparation of the zirconium silicate grinding ball at low temperature. The material powder is shaped to be biscuit balls for sintering to obtain compact, wear-resistant and high-strength zirconium silicon substrate grinding balls.

Description

technical field [0001] The invention relates to a grinding medium-low-temperature sintered zirconium silicate grinding ball, and provides a preparation method of the grinding ball. Background technique [0002] Grinding balls are widely used in mining, metallurgy, chemical industry, food, building materials and other industries to pulverize and mix raw materials through various methods such as collision, friction, rolling and extrusion of grinding balls. The quality of grinding balls seriously affects production efficiency and product quality. [0003] In recent years, the rapid development of ultra-fine powder technology and the development and utilization of low-grade minerals have greatly promoted the development and production of grinding ball media. Commonly used grinding media are steel, quartz, glass, alumina, zirconia, etc. Zirconia has good specific gravity and is a high-end grinding material, but its price is relatively high, while the grinding efficiency of othe...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/16C04B35/622C09K3/14
Inventor 王俊甫李强王柏昆周雄宋书明廖建中
Owner 江苏金石研磨有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap