Optical Adhesive Sheet
An adhesive sheet, optical technology, applied in the direction of adhesive type, ester copolymer adhesive, film/sheet adhesive, etc., can solve problems such as misoperation and achieve the effect of preventing misoperation
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Embodiment 1
[0097] (Preparation of photopolymerizable composition)
[0098] 40 parts by weight of 2-ethylhexyl acrylate, 59 parts by weight of 2-methoxyethyl acrylate, 1 part by weight of 4-hydroxybutyl acrylate, 0.05 parts by weight of 2,2-dimethoxy-1 , 2-diphenyl-1-ketone (trade name "Irugakuyua 651", manufactured by Ciba Corporation of Japan) and 0.05 parts by weight of 1-hydroxycyclohexyl-phenyl ketone (trade name "Irugakuyua 184", manufactured by Ciba Corporation of Japan ) into a four-necked flask, and carried out partial photopolymerization by exposing to ultraviolet rays under a nitrogen atmosphere, thereby obtaining a partial polymer (monomer slurry) with a polymerization rate of 10%.
[0099] After adding 0.1 part by weight of an isocyanate compound (trade name "Corone-to L", manufactured by Nippon Polyurethane Industry Co., Ltd., solid content ratio: 75% by weight) in terms of solid content to 100 parts by weight of this part of the polymer, it was uniformly mixed. Mix to prep...
Embodiment 2
[0103] (Preparation of photopolymerizable composition)
[0104] 69 parts by weight of 2-ethylhexyl acrylate, 30 parts by weight of 2-methoxyethyl acrylate, 1 part by weight of 4-hydroxybutyl acrylate, 3 parts by weight of acrylic acid, 0.05 parts by weight of 2,2-di Methoxy-1,2-diphenyl-1-one (trade name "Irugakuyua 651", manufactured by Ciba Corporation of Japan) and 0.05 parts by weight of 1-hydroxycyclohexyl-phenyl ketone (trade name "Irugakuyua 184", (manufactured by Ciba Co., Ltd. Japan) was charged into a four-necked flask, and subjected to partial photopolymerization by exposure to ultraviolet rays under a nitrogen atmosphere, thereby obtaining a partial polymer (monomer slurry) with a polymerization rate of 10%.
[0105] After adding 0.01 weight part of trimethylolpropane triacrylate to 100 weight part of this partial polymer, this was mixed uniformly, and the photopolymerizable composition was prepared.
[0106] (production of adhesive sheet)
[0107] On the release...
Embodiment 3
[0109] (Preparation of photopolymerizable composition)
[0110] 68 parts by weight of 2-ethylhexyl acrylate, 24 parts by weight of 2-methoxyethyl acrylate, 6 parts by weight of N-vinylpyrrolidone, 2 parts by weight of hydroxyethylacrylamide, 0.05 parts by weight of 2,2 - Dimethoxy-1,2-diphenyl-1-ketone (trade name "Irugakuyua 651", manufactured by Ciba Corporation of Japan) and 0.05 parts by weight of 1-hydroxycyclohexyl-phenylketone (tradename "Irugakuyua 184" ", manufactured by Ciba Corporation of Japan) was added in a four-necked flask, and carried out partial photopolymerization by being exposed to ultraviolet rays under a nitrogen atmosphere, thereby obtaining a partial polymer (monomer slurry) with a polymerization rate of 10%.
[0111] After adding 0.015 weight part of trimethylolpropane triacrylates to 100 weight part of polymers of this part, this was mixed uniformly, and the photopolymerizable composition was prepared.
[0112] (production of adhesive sheet)
[0113]...
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Abstract
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