Method for forming coating on inner surface of polycrystalline silicon ingot casting crucible
A polycrystalline silicon and crucible technology is applied to form a coating on the inner surface of a crucible for polycrystalline silicon ingots, and in the field of crucibles for polycrystalline silicon ingots, it can solve the problems of coating erosion, easy falling off, and high energy consumption, and achieve the effect of saving energy
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Embodiment 1
[0027] A coating is formed on the inner surface of a quartz crucible according to the following steps, thereby obtaining a crucible for polysilicon ingot comprising a coating formed using the method according to the present invention
[0028] 1) Weigh 400g of silicon nitride powder, add 1600g of pure water to it, stir and disperse evenly to prepare a coating composition;
[0029] 2) Place the quartz crucible on the heating device, heat it to 80°C and keep it warm;
[0030] 3) the coating composition prepared in the above step 1) is used to make it form a coating with a thickness of 300 microns on the inner surface of the quartz crucible by a brushing method; before this, calculate the position of the silicon melt level , when painting, it is necessary to apply multiple times within the range of 50 mm above and below the liquid surface to make the coating here thicker, and the thickness after drying here is 500 microns;
[0031] 4) Dry the coated quartz crucible in an aerobic ...
Embodiment 2
[0033] Except that 20 g of methanol was added in step 1), and the drying temperature in step 4) was 100° C., a polysilicon casting containing a coating formed by the method according to the present invention was obtained in the same steps as in Example 1. Crucible for ingot.
Embodiment 3
[0035] Except that 15 g of acrylic acid was added in step 1), and the drying temperature in step 4) was 100° C., a polysilicon casting containing a coating formed by the method according to the present invention was obtained in the same steps as in Example 1. Crucible for ingot.
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