Preparation method of spherical composite humidity-controlling material
A humidity-conditioning material and spherical technology, which is applied in the field of preparation of humidity-conditioning materials, can solve the problems of insufficient number of pores and insufficient specific surface area, and achieve the effects of large specific surface area, fast moisture absorption rate, and improved wet capacity.
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Embodiment 1
[0017] Embodiment 1: a kind of preparation method of spherical composite humidity control material is characterized in that the steps are as follows:
[0018] a. activating halloysite at 450° C. for 2 hours to obtain activated halloysite;
[0019] b. Take 30 parts of polyacrylic acid in parts by mass, add to 115 parts of sodium hydroxide solution (dissolve 15 parts of sodium hydroxide in 100 parts of distilled water) for neutralization, and then take 0.9 parts of konjac glucomannan by parts by mass , 3 parts of activated halloysite, 0.3 parts of potassium persulfate, 0.3 parts of N,N'-methylenebisacrylamide, aluminum chloride solution made of 0.3 parts of aluminum chloride and 10 parts of water, respectively added Put it into the reactor filled with the above-mentioned neutralized solution (the solution obtained after neutralization of polyacrylic acid and sodium hydroxide solution), stir and react for 1 hour at a temperature of 70°C; the order of addition is: add persulfuric ...
Embodiment 2
[0023] Embodiment 2: a kind of preparation method of spherical composite humidity control material, it is characterized in that the steps are as follows:
[0024] a. activating halloysite at 450°C for 2.5 hours to obtain activated halloysite;
[0025] b. Take 30 parts of polyacrylic acid in parts by mass, add to 115 parts of sodium hydroxide solution (dissolve 15 parts of sodium hydroxide in 100 parts of distilled water) for neutralization, and then take 1.8 parts of konjac glucomannan in parts by mass , 4.5 parts of activated halloysite, 0.3 parts of potassium persulfate, 0.3 parts of N,N'-methylenebisacrylamide, aluminum chloride solution made of 0.9 parts of aluminum chloride and 10 parts of water, respectively added Put into the reactor filled with the above-mentioned neutralized solution (the solution obtained after neutralization of polyacrylic acid and sodium hydroxide solution), stir and react for 1.5 hours at a temperature of 75°C; the order of adding persulfuric acid...
Embodiment 3
[0029] Embodiment 3: a kind of preparation method of spherical composite humidity control material, it is characterized in that the steps are as follows:
[0030] a. activating halloysite at 450° C. for 3 hours to obtain activated halloysite;
[0031] b. Take 30 parts of polyacrylic acid in parts by mass, add to 115 parts of sodium hydroxide solution (dissolve 15 parts of sodium hydroxide in 100 parts of distilled water) for neutralization, and then take 2.7 parts of konjac glucomannan by parts by mass , 6 parts of activated halloysite, 0.3 parts of potassium persulfate, 0.3 parts of N,N'-methylenebisacrylamide, aluminum chloride solution made of 1.5 parts of aluminum chloride and 10 parts of water, respectively added Put into the reactor filled with the above-mentioned neutralized solution (the solution obtained after the neutralization of polyacrylic acid and sodium hydroxide solution), stir and react for 2 hours at a temperature of 80°C; the order of addition is: add persul...
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