Liquid nitrogen washing device with function of producing natural gas

A natural gas and liquid nitrogen washing technology, applied in the field of coal chemical industry, can solve the problems such as the liquid nitrogen washing device cannot operate normally, and achieve the effect of ensuring long-term stable operation and increasing business opportunities.

Active Publication Date: 2013-04-17
李红凯 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The object of the present invention is exactly to solve when CH in the purified syngas Content ≥ 1% or higher (as Lurgi pressurized gasification, KBR pressurized gasification, or other gasification methods etc. contain about 2 % (dry basis) and above methane), methane solidifies and freezes in the cold box of the liquid nitrogen washing device, causing the problem that the liquid nitrogen washing device cannot operate normally. It is a clean fuel - natural gas, which is called "LNG" (liquefied natural gas) after liquefaction

Method used

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  • Liquid nitrogen washing device with function of producing natural gas

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Embodiment 1

[0027] The purified syngas first enters the molecular sieve adsorber in the liquid nitrogen washing device, and the trace amount of CO contained in it 2 and CH 3 OH is adsorbed in the adsorber. Afterwards, the purified synthesis gas (3-001 stream) enters the first raw gas cooler in the "cold box", and is cooled to about -128°C by several reheated streams; then enters the second raw gas cooler and continues It is cooled to about -155°C by several reheated streams and drawn from the middle of the second raw material gas cooler, and sent to the middle of the demethanizer into the tower. At this time, the stream entering the tower is close to the bubble point state and contains a small amount of liquid phase: the gas phase flows to the top of the tower, and the liquid phase flows to the bottom of the tower.

[0028] The bottom fraction (i.e. natural gas) enters the bottom fraction separator after decompression, and the separated gas / liquid two-phase, that is, the cooler, reheats...

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Abstract

The invention discloses a liquid nitrogen washing device with a function of producing natural gas, which comprises a first feed gas cooler 1, a second feed gas cooler 2, a nitrogen washing tower 3, a purifying synthesis gas pipe and a demethanizer 3, wherein the purifying synthesis gas pipe runs through the first feed gas cooler 1 and the second feed gas cooler 2 in sequence; the demethanizer 3 is provided with an air inlet end, an air outlet end and a fraction output end; the purifying synthesis gas pipe is communicated with the air inlet end after running through the second feed gas cooler; and the air outlet end is communicated with the nitrogen washing tower 3 through a pipe. The liquid nitrogen washing device with the function of producing natural gas is capable of recycling methane generated during the process of coal gasification and manufacturing the methane into natural gas, which not only realizes the goal of obtaining clean natural gas containing about 99% of methane while producing refined ammonia synthesis gas, but also adds a new product variety and increases the business opportunity of a factory.

Description

technical field [0001] The invention relates to the field of coal chemical industry, and relates to a synthesis gas refining process for producing synthetic ammonia, in particular to a liquid nitrogen washing device for concurrently producing natural gas. Background technique [0002] Coal is passed through the gasification section to obtain crude gas, and the crude gas enters the low-temperature methanol washing device after the transformation section, and the purified synthesis gas is obtained after the acid gas is removed in the low-temperature methanol washing device, and the purified syngas enters the liquid nitrogen washing device to remove trace CO, etc. Synthetic gas, the raw material for synthetic ammonia, is obtained. [0003] At present, the domestic "liquid nitrogen washing device" used in the field of coal chemical industry to produce synthetic ammonia and refine syngas is all used to remove and purify CO in syngas. But while washing off CO, CH 4 and Ar are al...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B3/52
Inventor 李红凯薛天祥葛雄
Owner 李红凯
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