Method for producing needle coke by catalytic cracking-delayed coking combination process

A delayed coking and catalytic cracking technology, which is applied in the field of needle coke production by catalytic cracking-delayed coking combined process, can solve the problem of heavy oil aromatics treatment process without further explanation, without paying attention to the full growth of mesophase, tensile deformation, increase Regenerator load, etc.

Active Publication Date: 2013-04-17
CHINA PETROLEUM & CHEM CORP +1
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AI Technical Summary

Problems solved by technology

Catalytic cracking heavy cycle oil is rich in aromatics, and aromatics are non-ideal feedstocks for catalytic cracking. Therefore, this method allows heavy aromatics to circulate continuously in the catalytic cracking unit, which will inevitably result in low yield of light oil, large amount of coke, and increased The regenerator load reduces the processing capacity and economic benefits of the heavy oil catalytic cracking unit
[0003] CN1133338A discloses a combined process for producing high-quality catalytic cracking raw materials, which combines coking and lubricating oil extraction devices, and extracts coking wax oil with lubricating oil extract, so that the alkali nitrogen and colloid content of coking wax oil is greatly reduced. To provide high-quality raw materials for the catalytic cracking unit, this method recycles the coking of the extracted oil rich in aromatics, and only produces ordinary coke out of the unit, so that it has not been effectively utilized
[0004] CN87107146A discloses catalytic cracking-catalytic heavy ...

Method used

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Embodiment 1

[0020] Firstly, the feedstock oil enters the catalytic cracking unit for catalytic cracking. The specific properties of the feedstock oil are shown in Table 1. Conventional ZSM-5 molecular sieves are used for catalytic cracking. The process conditions of the catalytic cracking unit are shown in Table 2. The catalytic cracking products enter the fractionation tower to separate the gas, gasoline fraction, diesel fraction and catalytic oil slurry, recover the gas, gasoline fraction and diesel fraction, and the catalytic oil slurry is filtered and then sent to the delayed coking unit. The temperature of the heating furnace of the delayed coking unit is operated at variable temperature. The temperature range is 430~520°C. The operating conditions of the coking tower are shown in Table 2. When the processing capacity of the delayed coking device reaches 70% of its total processing capacity, the process in step (1) The resulting oil is separated into gas and gasoline fractions, and th...

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Abstract

The invention discloses a method for producing needle coke by a catalytic cracking-delayed coking combination process, which comprises steps as follows: (1) raw oil enters a catalytic cracking unit to be subjected to catalytic cracking reaction, and generated oil enters a fractionating tower to be separated into gas, gasoline fraction diesel fraction and catalytic slurry oil; (2) the catalytic slurry oil obtained in the step (1) is filtered and enters a delayed coker, when the treatment amount of the delayed coker reaches 60-80% of the total treatment amount, the generated oil in the step (1) is separated to obtain gas and gasoline fraction, and the rest fraction is filtered to totally enter the delayed coker; and (3) when reaching the total treatment amount of the delayed coker, oil introduction is stopped, and the coke tower is switched to perform the coking scorching stage, so that the needle coke deposits on the tower bottom. The method can obtain the high-fiber-structure good-quality needle coke product while obtaining qualified catalytic cracking products.

Description

technical field [0001] The invention relates to a method for producing needle coke by a combination process of catalytic cracking and delayed coking. Background technique [0002] Catalytic cracking is an important heavy oil processing method. The traditional processing method for the heavy cycle oil obtained in the catalytic cracking process is mainly full or partial re-refining, and the re-refining ratio is generally 0.3~0.7. Catalytic cracking heavy cycle oil is rich in aromatics, and aromatics are non-ideal feedstocks for catalytic cracking. Therefore, this method allows heavy aromatics to circulate continuously in the catalytic cracking unit, which will inevitably result in low yield of light oil, large amount of coke, and increased The regenerator load reduces the processing capacity and economic benefits of the heavy oil catalytic cracking unit. [0003] CN1133338A discloses a combined process for producing high-quality catalytic cracking raw materials, which combine...

Claims

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Application Information

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IPC IPC(8): C10G55/06
Inventor 初人庆蒋立敬杜正军勾连忠矫德卫张学萍
Owner CHINA PETROLEUM & CHEM CORP
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