Unlock instant, AI-driven research and patent intelligence for your innovation.

Method for treating sump oil of coal tar

A processing method and technology for coal tar, applied in the field of coal chemical industry, can solve the problems of waste of coal tar resources and no treatment, and achieve the effects of low cost, resource saving and low investment

Active Publication Date: 2013-06-19
王树宽
View PDF3 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In actual production, coal tar waste oil is burned as fuel without further treatment, resulting in waste of coal tar resources

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Taking the treatment of 1000g of coal tar waste oil as an example, the treatment method consists of the following steps:

[0014] (1) Add 1000g of coal tar waste oil to the mixing kettle, which contains 60% of coal tar, 30% of water and 10% of quinoline insoluble matter, and then add 1500g of benzene, 120g of sodium carbonate and 100g of WF- Type 01 demulsifier (produced by Shaanxi Zhongheng Energy Technology Co., Ltd.), the mass ratio of coal tar waste oil to benzene, sodium carbonate, and WF-01 type demulsifier is 1:1.5:0.12:0.1, under normal pressure and 60°C Stir for 38 minutes to make it evenly mixed;

[0015] (2) Stand still in the mixing tank for 35 minutes, layering, so that the quinoline insoluble matter in the coal tar waste oil is deposited in the water, discharged from the outlet at the bottom of the mixing tank, and sent to the sewage station for treatment, the upper part of the mixing tank contains coal The mixture of tar, benzene and a small amount of wa...

Embodiment 2

[0017] Taking the treatment of 1000g of coal tar waste oil as an example, the treatment method consists of the following steps:

[0018] (1) Add 1000g of coal tar waste oil to the mixing kettle, which contains 60% of coal tar, 30% of water and 10% of quinoline insoluble matter, and then add 1500g of benzene, 200g of sodium carbonate and 200g of WF into the mixing kettle -01 type demulsifier, the mass ratio of coal tar waste oil to benzene, sodium carbonate, WF-01 type demulsifier is 1:1.5:0.2:0.2, stir for 38min under normal pressure and 60°C to make it evenly mixed;

[0019] Step (2) is the same as in Example 1, benzene and water are distilled from the top of the still, and the benzene is recovered for recycling. Coal tar is output from the bottom outlet of the still, recovered, and processed in the next step. The recovery rate of coal tar is 98%.

Embodiment 3

[0021] Taking the treatment of 1000g of coal tar waste oil as an example, the treatment method consists of the following steps:

[0022] (1) Add 1000g of coal tar waste oil into the mixing kettle, which contains 60% of coal tar, 30% of water and 10% of quinoline insoluble matter, and then add 1200g of benzene, 200g of sodium carbonate and 200g of WF into the mixing kettle -01 type demulsifier, the mass ratio of coal tar waste oil to benzene, sodium carbonate, WF-01 type demulsifier is 1:1.2:0.2:0.2, stir for 38min under normal pressure and 60°C to make it evenly mixed;

[0023] Step (2) is the same as in Example 1, benzene and water are distilled from the top of the still, and the benzene is recovered for recycling. Coal tar is output from the bottom outlet of the still, recovered, and processed in the next step. The recovery rate of coal tar was 97.7%.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
recovery rateaaaaaaaaaa
recovery rateaaaaaaaaaa
recovery rateaaaaaaaaaa
Login to View More

Abstract

The invention relates to a method for treating sump oil of coal tar. The method comprises the following steps of: separating quinoline insoluble from other components in sump oil by utilizing benzene, sodium carbonate and WF-01 type demulsifier; and further distilling benzene and water out of sump oil; separating and recycling coal tar. Therefore, the effective component coal tar in the sump oil can be effectively extracted and recycled with the recycling rate being 95 percent, so that the method saves coal tar resources, is simple in treatment process, low in investment, low in cost and safe and stable in production operation, and further improves the economical benefit of production.

Description

technical field [0001] The invention belongs to the field of coal chemical industry, and in particular relates to a method for recycling waste oil produced in the coal tar pretreatment process. Background technique [0002] my country is a country that is "short of oil, less gas, and relatively rich in coal resources". In recent years, driven by high oil prices, my country's coal tar hydrogenation to fuel oil industry has developed rapidly, and coal tar has replaced petroleum , the production of fuel oil products through catalytic hydrogenation has certain significance for alleviating the shortage of oil supply in my country. In the process of catalytic hydrogenation of coal tar to produce fuel oil, the coal tar needs to be pretreated first. The pretreatment methods currently used are: centrifugal separation, automatic backwash filtration, etc. However, a certain amount of coal tar oil will be produced during the pretreatment process of slag removal. Coal tar waste oil is m...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C10G53/02
Inventor 杨占彪王树宽
Owner 王树宽